4-(2-BroMoethyl)Morpholine HydrobroMide

Base Information

• Chemical Name: 4-(2-BroMoethyl)Morpholine HydrobroMide
• CAS No.: 42802-94-8
• Molecular Formula: C6H12 Br N O . Br H
• Molecular Weight: 274.983
• Hs Code.: 2934999090
• Mol file: 42802-94-8.mol

Synonyms:Morpholine,4-(2-bromoethyl)-, hydrobromide (9CI); b-Morpholinoethylbromide hydrobromide

Chemical Property of 4-(2-BroMoethyl)Morpholine HydrobroMide

Chemical Property:

• Melting Point: 222-224℃ (methanol )
• PSA: 12.47000
• LogP: 1.60950
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

99%, ^*data from raw suppliers

4-(2-Bromoethyl)morpholineHydrobromide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(2-BroMoethyl)Morpholine HydrobroMide

There total 1 articles about 4-(2-BroMoethyl)Morpholine HydrobroMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

2-(morpholin-4-yl)ethanol (622-40-2) → 4-(2-bromoethyl)morpholine hydrobromide (42802-94-8)

Guidance literature:

With dibromotriphenylphosphorane; In dichloromethane; at 25 ℃; for 1h;

Reference yield: 81.1%

4-(2-bromoethyl)morpholine hydrobromide (42802-94-8) + methyl 4-((2-(4-hydroxyphenyl)isonicotinamido)methyl)benzoate → methyl 4-((2-(4-(2-morpholinylethoxy)phenyl)isonicotinamido)methyl)benzoate

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 1h;

Reference yield: 79.0%

N'-((5-cyanopyrazolo[1,5-a]pyridin-3-yl)methylene)-2-methyl-5-nitrobenzenesulfonohydrazide (1101118-71-1) + 4-(2-bromoethyl)morpholine hydrobromide (42802-94-8) → N'-((5-cyanopyrazolo[1,5-a]pyridin-3-yl)methylene)-2-methyl-N-(2-morpholinoethyl)-5-nitrobenzenesulfonohydrazide (1101118-81-3)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

DOI:10.1016/j.bmc.2011.11.031

upstream raw materials:

2-(morpholin-4-yl)ethanol

Downstream raw materials:

N-(2-morpholinoethyl)aniline

N'-((5-cyanopyrazolo[1,5-a]pyridin-3-yl)methylene)-2-methyl-N-(2-morpholinoethyl)-5-nitrobenzenesulfonohydrazide

6,6-dimethyl-2-{2-[(1-methyl-1H-pyrazol-5-yl)amino]pyrimidin-4-yl}-5-[2-(morpholin-4-yl)ethyl]-5,6-dihydro-4H-thieno[2,3-c]pyrrol-4-one

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