(4E,6E)-6-Phenyl-bicyclo[9.2.2]pentadeca-1⁽¹⁴⁾,4,6,11⁽¹⁵⁾,12-pentaene-2,2,10,10-tetracarbonitrile

Base Information

• Chemical Name: (4E,6E)-6-Phenyl-bicyclo[9.2.2]pentadeca-1⁽¹⁴⁾,4,6,11⁽¹⁵⁾,12-pentaene-2,2,10,10-tetracarbonitrile
• CAS No.: 68326-80-7
• Molecular Formula: C₂₅H₁₈N₄
• Molecular Weight: 374.445

Synonyms:(4E,6E)-6-Phenyl-bicyclo[9.2.2]pentadeca-1⁽¹⁴⁾,4,6,11⁽¹⁵⁾,12-pentaene-2,2,10,10-tetracarbonitrile

Chemical Property of (4E,6E)-6-Phenyl-bicyclo[9.2.2]pentadeca-1⁽¹⁴⁾,4,6,11⁽¹⁵⁾,12-pentaene-2,2,10,10-tetracarbonitrile

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Technology Process of (4E,6E)-6-Phenyl-bicyclo[9.2.2]pentadeca-1⁽¹⁴⁾,4,6,11⁽¹⁵⁾,12-pentaene-2,2,10,10-tetracarbonitrile

There total 3 articles about (4E,6E)-6-Phenyl-bicyclo[9.2.2]pentadeca-1⁽¹⁴⁾,4,6,11⁽¹⁵⁾,12-pentaene-2,2,10,10-tetracarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

(Z)-1-cyclopropyl-1-phenyl-1,3-butadiene (1258388-49-6) + 7,7',8,8'-tetracyanoquinodimethane (1518-16-7,6144-37-2) → (4E,6E)-6-Phenyl-bicyclo[9.2.2]pentadeca-1(14),4,6,11(15),12-pentaene-2,2,10,10-tetracarbonitrile (68326-80-7)

Guidance literature:

With hydroquinone; In dichloromethane; for 50h; Ambient temperature;

DOI:10.1021/ja00413a017

Reference yield: 61.0%

(E)-(1-cyclopropylbuta-1,3-dienyl)benzene (68326-79-4) + 7,7',8,8'-tetracyanoquinodimethane (1518-16-7,6144-37-2) → (4E,6E)-6-Phenyl-bicyclo[9.2.2]pentadeca-1(14),4,6,11(15),12-pentaene-2,2,10,10-tetracarbonitrile (68326-80-7)

Guidance literature:

With hydroquinone; In dichloromethane; Ambient temperature;

DOI:10.1021/ja00413a017

Reference yield:

→ (4E,6E)-6-Phenyl-bicyclo[9.2.2]pentadeca-1(14),4,6,11(15),12-pentaene-2,2,10,10-tetracarbonitrile (68326-80-7)

Guidance literature:

TCNQ, Cyclopropylbutadien E-1d;

DOI:10.1246/cl.1978.1053

upstream raw materials:

(Z)-1-cyclopropyl-1-phenyl-1,3-butadiene

7,7',8,8'-tetracyanoquinodimethane

(E)-(1-cyclopropylbuta-1,3-dienyl)benzene

Downstream raw materials:

5-phenyl-1-p-tolyloctane

5-phenyl-1-p-tolyl-2-octene

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