p-iodophenylbuta-1,3-diynyl methyl sulfide

Base Information

Chemical Name:p-iodophenylbuta-1,3-diynyl methyl sulfide
CAS No.:1276057-40-9
Molecular Formula:C₁₁H₇IS
Molecular Weight:298.147
Hs Code.:

Synonyms:p-iodophenylbuta-1,3-diynyl methyl sulfide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-iodophenylbuta-1,3-diynyl methyl sulfide

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Technology Process of p-iodophenylbuta-1,3-diynyl methyl sulfide

There total 5 articles about p-iodophenylbuta-1,3-diynyl methyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1446871-32-4
(E)-1-methylthio-1-phenylsulphonyl-(4-(4-iodo)phenyl)-1-butene-3-yne

: 1276057-40-9
p-iodophenylbuta-1,3-diynyl methyl sulfide

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; Inert atmosphere;
DOI:10.1080/00397911.2012.729280

Reference yield: 79.0%

: C₁₁H₁₁IO₂S

: 1276057-40-9
p-iodophenylbuta-1,3-diynyl methyl sulfide

Guidance literature:: C₁₁H₁₁IO₂S; With lithium hexamethyldisilazane; In tetrahydrofuran; ethylbenzene; at -78 ℃; for 0.5h; Inert atmosphere;

With diethyl chlorophosphate; In tetrahydrofuran; ethylbenzene; at -78 - 20 ℃; for 0.5h; Inert atmosphere;

With lithium hexamethyldisilazane; In tetrahydrofuran; ethylbenzene; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.1002/hc.21280

Reference yield:

: C₂₁H₂₄IO₆PS₂

: 1276057-40-9
p-iodophenylbuta-1,3-diynyl methyl sulfide

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;
DOI:10.1080/00397911.2012.729280