6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-trityl-1H-benzotriazole

Base Information

Chemical Name:6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-trityl-1H-benzotriazole
CAS No.:1365803-27-5
Molecular Formula:C₃₁H₃₀BN₃O₂
Molecular Weight:487.409
Hs Code.:

Synonyms:6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-trityl-1H-benzotriazole

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Chemical Property of 6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-trityl-1H-benzotriazole

Chemical Property:

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Technology Process of 6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-trityl-1H-benzotriazole

There total 1 articles about 6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-trityl-1H-benzotriazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1257651-13-0
6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-benzo[d][1,2,3]triazole

: 76-83-5
trityl chloride

: 1365803-27-5
6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-trityl-1H-benzotriazole

Guidance literature:: With triethylamine; In acetonitrile;

Reference yield: 77.0%

: 1365802-96-5
N-[3,5-bis(trifluoromethyl)phenyl]-4-chlorophthalazin-1-amine

: 1365803-27-5
6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-trityl-1H-benzotriazole

: 1365803-28-6
N-[3,5-bis(trifluoromethyl)phenyl]-4-(1-trityl-1H-benzotriazol-6-yl)phthalazin-1-amine

Guidance literature:: With potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; water; at 110 ℃; for 0.333333h; microwave irradiation;

Reference yield:

: 1365802-96-5
N-[3,5-bis(trifluoromethyl)phenyl]-4-chlorophthalazin-1-amine

: 1365803-27-5
6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-trityl-1H-benzotriazole

: 1365802-75-0
4-(1H-1,2,3-benzotriazol-6-yl)-N-[3,5-bis(trifluoromethyl)phenyl]phthalazin-1-amine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium phosphate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 0.33 h / 110 °C / microwave irradiation

2: hydrogenchloride / diethyl ether; methanol / 1 h

With hydrogenchloride; potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; methanol; diethyl ether; water;