N-<3-(Trifluoromethyl)phenyl>-P-(α-chloro-2-tolyl)-P-methylphosphinamide

Base Information

Chemical Name:N-<3-(Trifluoromethyl)phenyl>-P-(α-chloro-2-tolyl)-P-methylphosphinamide
CAS No.:78089-70-0
Molecular Formula:C₁₅H₁₄ClF₃NOP
Molecular Weight:347.704
Hs Code.:

Synonyms:N-<3-(Trifluoromethyl)phenyl>-P-(α-chloro-2-tolyl)-P-methylphosphinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<3-(Trifluoromethyl)phenyl>-P-(α-chloro-2-tolyl)-P-methylphosphinamide

Chemical Property:

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Technology Process of N-<3-(Trifluoromethyl)phenyl>-P-(α-chloro-2-tolyl)-P-methylphosphinamide

There total 4 articles about N-<3-(Trifluoromethyl)phenyl>-P-(α-chloro-2-tolyl)-P-methylphosphinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 615-37-2
ortho-methylphenyl iodide

: 78089-70-0
N-<3-(Trifluoromethyl)phenyl>-P-(α-chloro-2-tolyl)-P-methylphosphinamide

Guidance literature:: Multi-step reaction with 4 steps

1: NiCl₂ / 2.5 h / 160 - 170 °C

2: PCl₅ / benzene / 1 h / Heating

3: Cl₂ / CCl₄ / 1.5 h / Heating; Irradiation

4: diethyl ether

With phosphorus pentachloride; chlorine; nickel dichloride; In tetrachloromethane; diethyl ether; benzene;
DOI:10.1021/jo00330a021

Reference yield:

: 61820-30-2
ethyl methyl-o-tolylphosphinate

: 78089-70-0
N-<3-(Trifluoromethyl)phenyl>-P-(α-chloro-2-tolyl)-P-methylphosphinamide

Guidance literature:: Multi-step reaction with 3 steps

1: PCl₅ / benzene / 1 h / Heating

2: Cl₂ / CCl₄ / 1.5 h / Heating; Irradiation

3: diethyl ether

With phosphorus pentachloride; chlorine; In tetrachloromethane; diethyl ether; benzene;
DOI:10.1021/jo00330a021

Reference yield:

: 78089-64-2
Methyl(2-tolyl)phosphinyl Chloride

: 78089-70-0
N-<3-(Trifluoromethyl)phenyl>-P-(α-chloro-2-tolyl)-P-methylphosphinamide

Guidance literature:: Multi-step reaction with 2 steps

1: Cl₂ / CCl₄ / 1.5 h / Heating; Irradiation

2: diethyl ether

With chlorine; In tetrachloromethane; diethyl ether;
DOI:10.1021/jo00330a021