1'-dimethylaminomethyl-1-lithiumruthenocenide

Base Information

Chemical Name:1'-dimethylaminomethyl-1-lithiumruthenocenide
CAS No.:881171-94-4
Molecular Formula:C₁₃H₁₆LiNRu
Molecular Weight:294.288
Hs Code.:

Synonyms:1'-dimethylaminomethyl-1-lithiumruthenocenide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1'-dimethylaminomethyl-1-lithiumruthenocenide

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Technology Process of 1'-dimethylaminomethyl-1-lithiumruthenocenide

There total 1 articles about 1'-dimethylaminomethyl-1-lithiumruthenocenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-72-8,29786-93-4
n-butyllithium

: 881171-93-3
1'-dimethylaminomethyl-1-tri-n-butylstannylruthenocene

: 881171-94-4
1'-dimethylaminomethyl-1-lithiumruthenocenide

: 1461-25-2
tetra-n-butyltin(IV)

Guidance literature:: In tetrahydrofuran; hexane; under N2 atm.; soln. of n-BuLi in hexane was added to soln. of complex in THF at -78°C in H-type Schlenk tube; mixt. stirred for 30 min at -78°C; several drops of BuLi in hexane were added; volatiles evapd. (vac.); pentane distd. onto mixt.; mixt. was stripped with pentane by distg. pentane onto the mixt. and evapg. in vac.; mixt. washed (pentane); volatiles removed (vac.);
DOI:10.1016/j.jorganchem.2005.10.034