4-((1-Cyclopropyl-1,3-dioxobutan-2-yl)oxy)-2,6-dimethylbenzonitrile

Base Information

Chemical Name:4-((1-Cyclopropyl-1,3-dioxobutan-2-yl)oxy)-2,6-dimethylbenzonitrile
CAS No.:913346-12-0
Molecular Formula:C₁₆H₁₇NO₃
Molecular Weight:271.316
Hs Code.:2926909090
Mol file:913346-12-0.mol

Synonyms:4-((1-CYCLOPROPYL-1,3-DIOXOBUTAN-2-YL)OXY)-2,6-DIMETHYLBENZONITRILE;

Suppliers and Price of 4-((1-Cyclopropyl-1,3-dioxobutan-2-yl)oxy)-2,6-dimethylbenzonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of 4-((1-Cyclopropyl-1,3-dioxobutan-2-yl)oxy)-2,6-dimethylbenzonitrile

Chemical Property:

Melting Point:118℃
Boiling Point:454.945 °C at 760 mmHg
Flash Point:198.367 °C
PSA：67.16000
Density:1.184g/cm³
LogP:2.49058

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 4-((1-Cyclopropyl-1,3-dioxobutan-2-yl)oxy)-2,6-dimethylbenzonitrile

There total 3 articles about 4-((1-Cyclopropyl-1,3-dioxobutan-2-yl)oxy)-2,6-dimethylbenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 21573-10-4
1-cyclopropyl-butane-1,3-dione

: 58537-99-8
4-hydroxy-2,6-dimethylbenzonitrile

: 913346-12-0
4-[1-(cyclopropylcarbonyl)-2-oxopropoxy]-2,6-dimethylbenzonitrile

: 1174495-39-6
C₂₅H₂₄N₂O₄

Guidance literature:: 1-cyclopropyl-butane-1,3-dione; With chloro-trimethyl-silane; In dichloromethane; at 0 - 5 ℃; for 0.5h; Inert atmosphere; Large scale reaction;

With N-chloro-succinimide; In dichloromethane; at 0 - 5 ℃; for 2.08333h; Inert atmosphere; Large scale reaction;

4-hydroxy-2,6-dimethylbenzonitrile; With N-ethyl-N,N-diisopropylamine; In acetonitrile; for 15.8333h; Reflux; Large scale reaction;
DOI:10.1021/op900110k

Reference yield: 33.0%

: 473924-31-1
2-chloro-1-cyclopropylbutane-1,3-dione

: 58537-99-8
4-hydroxy-2,6-dimethylbenzonitrile

: 913346-12-0
4-[1-(cyclopropylcarbonyl)-2-oxopropoxy]-2,6-dimethylbenzonitrile

Guidance literature:: 4-hydroxy-2,6-dimethylbenzonitrile; With caesium carbonate; In acetone; at 20 ℃; for 0.5h;

2-chloro-1-cyclopropylbutane-1,3-dione; In acetone; for 2h; Heating / reflux;

With acetic acid; In acetone; at 20 ℃;