2-(2-azido-7-(2,5-bis(tetrahydro-2H-pyran-2-yloxy)phenyl)heptyl)isoindoline-1,3-dione

Base Information

Chemical Name:2-(2-azido-7-(2,5-bis(tetrahydro-2H-pyran-2-yloxy)phenyl)heptyl)isoindoline-1,3-dione
CAS No.:1309932-13-5
Molecular Formula:C₃₁H₃₈N₄O₆
Molecular Weight:562.666
Hs Code.:

Synonyms:2-(2-azido-7-(2,5-bis(tetrahydro-2H-pyran-2-yloxy)phenyl)heptyl)isoindoline-1,3-dione

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Chemical Property of 2-(2-azido-7-(2,5-bis(tetrahydro-2H-pyran-2-yloxy)phenyl)heptyl)isoindoline-1,3-dione

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Technology Process of 2-(2-azido-7-(2,5-bis(tetrahydro-2H-pyran-2-yloxy)phenyl)heptyl)isoindoline-1,3-dione

There total 6 articles about 2-(2-azido-7-(2,5-bis(tetrahydro-2H-pyran-2-yloxy)phenyl)heptyl)isoindoline-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4117-09-3
7-bromo-hept-1-ene

: 1309932-13-5
2-(2-azido-7-(2,5-bis(tetrahydro-2H-pyran-2-yloxy)phenyl)heptyl)isoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 5 steps

1.1: tert.-butyl lithium / tetrahydrofuran / 0.75 h / 0 °C

1.2: 3 h

2.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 0 - 25 °C

3.1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 24 h / 90 °C

4.1: triethylamine / tetrahydrofuran / 3 h

5.1: sodium azide / N,N-dimethyl-formamide / 72 h / 110 °C

With sodium azide; tert.-butyl lithium; sodium hydrogencarbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja203198y

Reference yield:

: C₃₂H₄₁NO₉S

: 1309932-13-5
2-(2-azido-7-(2,5-bis(tetrahydro-2H-pyran-2-yloxy)phenyl)heptyl)isoindoline-1,3-dione

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 110 ℃; for 72h;
DOI:10.1021/ja203198y

Reference yield:

: 1309932-12-4
2,2'-(2-(5-(oxiran-2-yl)pentyl)-1,4-phenylene)bis(oxy)bis(tetrahydro-2H-pyran)

: 1309932-13-5
2-(2-azido-7-(2,5-bis(tetrahydro-2H-pyran-2-yloxy)phenyl)heptyl)isoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 24 h / 90 °C

2: triethylamine / tetrahydrofuran / 3 h

3: sodium azide / N,N-dimethyl-formamide / 72 h / 110 °C

With sodium azide; sodium hydrogencarbonate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ja203198y