ethyl 3-<4-<7-carbomethoxy-9-oxo-3-<3-<5-benzyloxy)-2-ethyl-4-phenylphenoxy>propoxy>-9H-xanthene>>propanoate

Base Information

Chemical Name:ethyl 3-<4-<7-carbomethoxy-9-oxo-3-<3-<5-benzyloxy)-2-ethyl-4-phenylphenoxy>propoxy>-9H-xanthene>>propanoate
CAS No.:171880-19-6
Molecular Formula:C₄₄H₄₂O₉
Molecular Weight:714.812
Hs Code.:

Synonyms:ethyl 3-<4-<7-carbomethoxy-9-oxo-3-<3-<5-benzyloxy)-2-ethyl-4-phenylphenoxy>propoxy>-9H-xanthene>>propanoate

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Chemical Property of ethyl 3-<4-<7-carbomethoxy-9-oxo-3-<3-<5-benzyloxy)-2-ethyl-4-phenylphenoxy>propoxy>-9H-xanthene>>propanoate

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Technology Process of ethyl 3-<4-<7-carbomethoxy-9-oxo-3-<3-<5-benzyloxy)-2-ethyl-4-phenylphenoxy>propoxy>-9H-xanthene>>propanoate

There total 5 articles about ethyl 3-<4-<7-carbomethoxy-9-oxo-3-<3-<5-benzyloxy)-2-ethyl-4-phenylphenoxy>propoxy>-9H-xanthene>>propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 135199-66-5
7-carbomethoxy-3-hydroxy-9-oxo-9H-xanthene-4-propanoic acid ethyl ester

: 2-Benzyloxy-5-ethyl-4-(3-iodo-propoxy)-biphenyl

: 171880-19-6
ethyl 3-<4-<7-carbomethoxy-9-oxo-3-<3-<5-benzyloxy)-2-ethyl-4-phenylphenoxy>propoxy>-9H-xanthene>>propanoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jm00076a030

Reference yield:

: 152609-59-1
1-benzyloxy-4-ethyl-3-(3-chloro-1-propyloxy)-benzene

: 171880-19-6
ethyl 3-<4-<7-carbomethoxy-9-oxo-3-<3-<5-benzyloxy)-2-ethyl-4-phenylphenoxy>propoxy>-9H-xanthene>>propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / N-bromosuccinimide / CCl₄ / 6 h / Ambient temperature

2: 80 percent / Pd(PPh₃)4, aq. Na₂CO₃ / ethanol; benzene / 16 h / Heating

3: K₂CO₃, KI, DMSO / butan-2-one / 18 h / Heating

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; potassium carbonate; dimethyl sulfoxide; potassium iodide; In tetrachloromethane; ethanol; butanone; benzene;
DOI:10.1021/jm00022a006

Reference yield:

: 29682-12-0
1-[4-(benzyloxy)-2-hydroxyphenyl]ethanone

: 171880-19-6
ethyl 3-<4-<7-carbomethoxy-9-oxo-3-<3-<5-benzyloxy)-2-ethyl-4-phenylphenoxy>propoxy>-9H-xanthene>>propanoate

Guidance literature:: Multi-step reaction with 5 steps

1: 82 percent / K₂CO₃ / dimethylsulfoxide; butan-2-one / 24 h / Heating

2: 69 percent / trifluoroacetic acid, triethylsilane / CCl₄ / 1.5 h / Ambient temperature

3: 73 percent / N-bromosuccinimide / CCl₄ / 6 h / Ambient temperature

4: 80 percent / Pd(PPh₃)4, aq. Na₂CO₃ / ethanol; benzene / 16 h / Heating

5: K₂CO₃, KI, DMSO / butan-2-one / 18 h / Heating

With triethylsilane; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; potassium carbonate; dimethyl sulfoxide; trifluoroacetic acid; potassium iodide; In tetrachloromethane; ethanol; dimethyl sulfoxide; butanone; benzene;
DOI:10.1021/jm00022a006