1-O-methyl 2,3,4-tri-O-[6-(4-cyanobiphenyl-4'-yloxy)hexanoyl]-α-D-glucopyranuronic acid

Base Information

Chemical Name:1-O-methyl 2,3,4-tri-O-[6-(4-cyanobiphenyl-4'-yloxy)hexanoyl]-α-D-glucopyranuronic acid
CAS No.:1379595-11-5
Molecular Formula:C₆₄H₆₃N₃O₁₃
Molecular Weight:1082.22
Hs Code.:

Synonyms:1-O-methyl 2,3,4-tri-O-[6-(4-cyanobiphenyl-4'-yloxy)hexanoyl]-α-D-glucopyranuronic acid

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Chemical Property of 1-O-methyl 2,3,4-tri-O-[6-(4-cyanobiphenyl-4'-yloxy)hexanoyl]-α-D-glucopyranuronic acid

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Technology Process of 1-O-methyl 2,3,4-tri-O-[6-(4-cyanobiphenyl-4'-yloxy)hexanoyl]-α-D-glucopyranuronic acid

There total 8 articles about 1-O-methyl 2,3,4-tri-O-[6-(4-cyanobiphenyl-4'-yloxy)hexanoyl]-α-D-glucopyranuronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1379595-09-1
methyl 2,3,4-tri-O-[6-(4-cyanobiphenyl-4'-yloxy)hexanoyl]-α-D-glucopyranoside

: 1379595-11-5
1-O-methyl 2,3,4-tri-O-[6-(4-cyanobiphenyl-4'-yloxy)hexanoyl]-α-D-glucopyranuronic acid

Guidance literature:: With Jones reagent; In acetone; at 20 ℃; for 1h;
DOI:10.1002/chem.201102193

Reference yield:

: 1379595-07-9
methyl 2,3,4-tri-O-[6-(4-cyanobiphenyl-4'-yloxy)hexanoyl]-6-O-tert-butyldimethylsilyl-α-D-glucopyranoside

: 1379595-11-5
1-O-methyl 2,3,4-tri-O-[6-(4-cyanobiphenyl-4'-yloxy)hexanoyl]-α-D-glucopyranuronic acid

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; iodine(I) bromide / dichloromethane / 20 °C

2: Jones reagent / acetone / 1 h / 20 °C

With methanol; Jones reagent; iodine(I) bromide; In dichloromethane; acetone;
DOI:10.1002/chem.201102193

Reference yield:

: 63734-12-3,74247-81-7,74247-82-8,74264-88-3
methyl 6-O-(tert-butyldimethylsilyl)-α-D-glucopyranoside

: 1379595-11-5
1-O-methyl 2,3,4-tri-O-[6-(4-cyanobiphenyl-4'-yloxy)hexanoyl]-α-D-glucopyranuronic acid

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 336 h / 20 °C

2: methanol; iodine(I) bromide / dichloromethane / 20 °C

3: Jones reagent / acetone / 1 h / 20 °C

With methanol; dmap; Jones reagent; iodine(I) bromide; dicyclohexyl-carbodiimide; In dichloromethane; acetone;
DOI:10.1002/chem.201102193