2,3,6,7-tetrakis[4-(boronatodiphenylphosphino)propylthio]tetrathiafulvalene

Base Information

Chemical Name:2,3,6,7-tetrakis[4-(boronatodiphenylphosphino)propylthio]tetrathiafulvalene
CAS No.:1178859-26-1
Molecular Formula:C₆₆H₇₆B₄P₄S₈
Molecular Weight:1293
Hs Code.:

Synonyms:2,3,6,7-tetrakis[4-(boronatodiphenylphosphino)propylthio]tetrathiafulvalene

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Chemical Property of 2,3,6,7-tetrakis[4-(boronatodiphenylphosphino)propylthio]tetrathiafulvalene

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Technology Process of 2,3,6,7-tetrakis[4-(boronatodiphenylphosphino)propylthio]tetrathiafulvalene

There total 1 articles about 2,3,6,7-tetrakis[4-(boronatodiphenylphosphino)propylthio]tetrathiafulvalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 329966-55-4
3-iodopropyl(diphenyl)phosphine-borane

: 132765-36-7
2,3,6,7-tetrakis(2-cyanoethylthio)tetrathiafulvalene

: 1178859-26-1
2,3,6,7-tetrakis[4-(boronatodiphenylphosphino)propylthio]tetrathiafulvalene

Guidance literature:: 2,3,6,7-tetrakis(2-cyanoethylthio)tetrathiafulvalene; With caesium carbonate; In water; N,N-dimethyl-formamide; at 70 ℃; for 3h; Inert atmosphere;

3-iodopropyl(diphenyl)phosphine-borane; In water; N,N-dimethyl-formamide; for 12h; Inert atmosphere;
DOI:10.1016/j.jorganchem.2009.04.006

Reference yield: 71.0%

: 1178859-26-1
2,3,6,7-tetrakis[4-(boronatodiphenylphosphino)propylthio]tetrathiafulvalene

: 1178859-24-9
2,3,6,7-tetrakis[3-diphenylphosphinopropylthio]tetrathiafulvalene

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In toluene; at 50 ℃; for 4 - 5h; Inert atmosphere;
DOI:10.1016/j.jorganchem.2009.04.006

Reference yield:

: 14515-95-8,56083-13-7
cis-(tungsten tetracarbonyl bipiperidine)

: 1178859-26-1
2,3,6,7-tetrakis[4-(boronatodiphenylphosphino)propylthio]tetrathiafulvalene

: [(W(CO)4)2(2,3,6,7-tetrakis(3-diphenylphosphinobutylthio)tetrathiafulvalene)]

Guidance literature:: With 1,4-diazabicyclo[2.2.2]octane; In not given; addn. of DABCO to soln. of (C3S2(S(CH2)3PPh2BH3)2)2; treatment with cis-W(CO)4(NHC5H10)2;
DOI:10.1016/j.jorganchem.2009.04.006