tert-butyl {(1S)-2-[(trans-4-azidocyclohexyl)oxy]-1-methylethyl}carbamate

Base Information

Chemical Name:tert-butyl {(1S)-2-[(trans-4-azidocyclohexyl)oxy]-1-methylethyl}carbamate
CAS No.:1344685-32-0
Molecular Formula:C₁₄H₂₆N₄O₃
Molecular Weight:298.385
Hs Code.:

Synonyms:tert-butyl {(1S)-2-[(trans-4-azidocyclohexyl)oxy]-1-methylethyl}carbamate

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Chemical Property of tert-butyl {(1S)-2-[(trans-4-azidocyclohexyl)oxy]-1-methylethyl}carbamate

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Technology Process of tert-butyl {(1S)-2-[(trans-4-azidocyclohexyl)oxy]-1-methylethyl}carbamate

There total 5 articles about tert-butyl {(1S)-2-[(trans-4-azidocyclohexyl)oxy]-1-methylethyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1344685-31-9
tert-butyl {(1S)-2-[(cis-4-hydroxycyclohexyl)oxy]-1-methylethyl}carbamate

: 1344685-32-0
tert-butyl {(1S)-2-[(trans-4-azidocyclohexyl)oxy]-1-methylethyl}carbamate

Guidance literature:: With di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; triphenylphosphine; In toluene; at 10 - 35 ℃; for 16h;

Reference yield:

: 3233-32-7
hydroquinone monoacetate

: 1344685-32-0
tert-butyl {(1S)-2-[(trans-4-azidocyclohexyl)oxy]-1-methylethyl}carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / toluene; tetrahydrofuran / 16 h / 0 - 35 °C

2: potassium carbonate / methanol / 72 h / 10 - 35 °C

3: hydrogen / 5% rhodium-on-charcoal / water; methanol / 3 h / 60 °C

4: triphenylphosphine; diphenyl phosphoryl azide; di-isopropyl azodicarboxylate / toluene / 16 h / 10 - 35 °C

With di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; hydrogen; potassium carbonate; triphenylphosphine; 5% rhodium-on-charcoal; In tetrahydrofuran; methanol; water; toluene;

Reference yield:

: 1344685-29-5
4-({(2S)-2-[(tert-butoxycarbonyl)amino]propyl}oxy)phenyl acetate

: 1344685-32-0
tert-butyl {(1S)-2-[(trans-4-azidocyclohexyl)oxy]-1-methylethyl}carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / methanol / 72 h / 10 - 35 °C

2: hydrogen / 5% rhodium-on-charcoal / water; methanol / 3 h / 60 °C

3: triphenylphosphine; diphenyl phosphoryl azide; di-isopropyl azodicarboxylate / toluene / 16 h / 10 - 35 °C

With di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; hydrogen; potassium carbonate; triphenylphosphine; 5% rhodium-on-charcoal; In methanol; water; toluene;