triethyl 8-(4-methoxyphenyl)-12-oxo-12H-isoindolo[2,1-a]perimidine-9,10,11-tricarboxylate

Base Information

Chemical Name:triethyl 8-(4-methoxyphenyl)-12-oxo-12H-isoindolo[2,1-a]perimidine-9,10,11-tricarboxylate
CAS No.:1315594-41-2
Molecular Formula:C₃₄H₂₈N₂O₈
Molecular Weight:592.605
Hs Code.:

Synonyms:triethyl 8-(4-methoxyphenyl)-12-oxo-12H-isoindolo[2,1-a]perimidine-9,10,11-tricarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of triethyl 8-(4-methoxyphenyl)-12-oxo-12H-isoindolo[2,1-a]perimidine-9,10,11-tricarboxylate

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Technology Process of triethyl 8-(4-methoxyphenyl)-12-oxo-12H-isoindolo[2,1-a]perimidine-9,10,11-tricarboxylate

There total 2 articles about triethyl 8-(4-methoxyphenyl)-12-oxo-12H-isoindolo[2,1-a]perimidine-9,10,11-tricarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1315594-33-2
1-(4-methoxyphenyl)-2-(1H-perimidin-2(3H)-ylidene)ethan-1-one

: 762-21-0
acetylenedicarboxylic acid diethyl ester

: 1315594-41-2
triethyl 8-(4-methoxyphenyl)-12-oxo-12H-isoindolo[2,1-a]perimidine-9,10,11-tricarboxylate

Guidance literature:: With dmap; In ethyl acetate; for 0.5h; Reflux;
DOI:10.1016/j.tet.2011.05.078

Reference yield:

: 2881-83-6
ethyl 4-methoxybenzoylacetate

: 1315594-41-2
triethyl 8-(4-methoxyphenyl)-12-oxo-12H-isoindolo[2,1-a]perimidine-9,10,11-tricarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / 5,5-dimethyl-1,3-cyclohexadiene / 5 h / Reflux

2: dmap / ethyl acetate / 0.5 h / Reflux

With dmap; toluene-4-sulfonic acid; In 5,5-dimethyl-1,3-cyclohexadiene; ethyl acetate;
DOI:10.1016/j.tet.2011.05.078