Mg[(C₆H₂(CH₃)3)3(C₄H₂NC)3CHC₄HN](C₆H₄)CC(C₆H₄)Zn[(C₄H₂NC)4(C₆H₂(CH₃)3)3]

Base Information

Chemical Name:Mg[(C₆H₂(CH₃)3)3(C₄H₂NC)3CHC₄HN](C₆H₄)CC(C₆H₄)Zn[(C₄H₂NC)4(C₆H₂(CH₃)3)3]
CAS No.:295804-38-5
Molecular Formula:C₁₀₈H₉₀MgN₈Zn
Molecular Weight:1589.65
Hs Code.:

Mg[(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)3(C<sub>4</sub>H<sub>2</sub>NC)3CHC<sub>4</sub>HN](C<sub>6</sub>H<sub>4</sub>)CC(C<sub>6</sub>H<sub>4</sub>)Zn[(C<sub>4</sub>H<sub>2</sub>NC)4(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)3]

Synonyms:Mg[(C₆H₂(CH₃)3)3(C₄H₂NC)3CHC₄HN](C₆H₄)CC(C₆H₄)Zn[(C₄H₂NC)4(C₆H₂(CH₃)3)3]

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Chemical Property of Mg[(C₆H₂(CH₃)3)3(C₄H₂NC)3CHC₄HN](C₆H₄)CC(C₆H₄)Zn[(C₄H₂NC)4(C₆H₂(CH₃)3)3]

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Technology Process of Mg[(C₆H₂(CH₃)3)3(C₄H₂NC)3CHC₄HN](C₆H₄)CC(C₆H₄)Zn[(C₄H₂NC)4(C₆H₂(CH₃)3)3]

There total 1 articles about Mg[(C₆H₂(CH₃)3)3(C₄H₂NC)3CHC₄HN](C₆H₄)CC(C₆H₄)Zn[(C₄H₂NC)4(C₆H₂(CH₃)3)3] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 150152-74-2
5,10,15-tris(2,4,6-trimethylphenyl)-20-(p-ethynylphenyl)porphyrinatozinc(II)

: 295804-35-2
Mg(II) 5,10,15-trimesityl-2-(4-iodophenyl)porphyrin

: 295804-38-5
Mg[(C₆H₂(CH₃)3)3(C₄H₂NC)3CHC₄HN](C₆H₄)CC(C₆H₄)Zn[(C₄H₂NC)4(C₆H₂(CH₃)3)3]

Guidance literature:: With tris-(o-tolyl)phosphine; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In triethylamine; toluene; (Ar); solvents added to mixt. of Mg complex, Zn complex, Pd catalyst and phosphine, kept at 37 °C for 15 h; evapn. column chromy (alumina, toluene/CHCl3, 1:1), evapn., preparativesize exclusion chromy (Bio-Rad Bio-Beads SX-1, toluene), evapn., columnchromy (alumina, toluene, toluene/CHCl3, 1:1);
DOI:10.1021/ja001031x

Reference yield:

: 295804-38-5
[Zn(NC₄H₂C)4(C₆H₂(CH₃)3)3](C₆H₄)C₂(C₆H₄)[Mg(NC₄H₂C)3CH(C₄HN)(C₆H₂(CH₃)3)3]

: [Zn(NC₄H₂C)4(C₆H₂(CH₃)3)3](C₆H₄)C₂(C₆H₄)[Mg(NC₄H₂C)3CH(C₄HN)(C₆H₂(CH₃)3)3]⁽¹⁺⁾

Guidance literature:: With tris(4-bromophenyl)aminium hexachloroantimonate; In methanol; dichloromethane; not isolated, detn. by visible spectroscopy;
DOI:10.1016/S0009-2614(01)00452-3