5-(2-cyanoethoxycarbonyl)-2,6-dimethyl-1,4-dihydro-3-carboxamido>-4-(3,4-methylenedioxyphenyl)pyridine

Base Information

Chemical Name:5-(2-cyanoethoxycarbonyl)-2,6-dimethyl-1,4-dihydro-3-carboxamido>-4-(3,4-methylenedioxyphenyl)pyridine
CAS No.:219553-62-5
Molecular Formula:C₃₆H₄₂N₄O₇
Molecular Weight:642.752
Hs Code.:

5-(2-cyanoethoxycarbonyl)-2,6-dimethyl-1,4-dihydro-3-<N-<3-(4-(ethoxycarbonyl)-4-phenylpiperidin-1-yl)propyl>carboxamido>-4-(3,4-methylenedioxyphenyl)pyridine

Synonyms:5-(2-cyanoethoxycarbonyl)-2,6-dimethyl-1,4-dihydro-3-carboxamido>-4-(3,4-methylenedioxyphenyl)pyridine

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Chemical Property of 5-(2-cyanoethoxycarbonyl)-2,6-dimethyl-1,4-dihydro-3-carboxamido>-4-(3,4-methylenedioxyphenyl)pyridine

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Technology Process of 5-(2-cyanoethoxycarbonyl)-2,6-dimethyl-1,4-dihydro-3-carboxamido>-4-(3,4-methylenedioxyphenyl)pyridine

There total 3 articles about 5-(2-cyanoethoxycarbonyl)-2,6-dimethyl-1,4-dihydro-3-carboxamido>-4-(3,4-methylenedioxyphenyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 219553-61-4
5-(2-cyanoethoxycarbonyl)-1,4-dihydro-2,6-dimethyl-4-(3,4-methylenedioxyphenyl)pyridine-3-carboxylic acid

: 166810-76-0
3-(4-Ethoxycarbonyl-4-phenylpiperidin-1-yl)-propylamine

: 219553-62-5
5-(2-cyanoethoxycarbonyl)-2,6-dimethyl-1,4-dihydro-3-carboxamido>-4-(3,4-methylenedioxyphenyl)pyridine

Guidance literature:: With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; for 14h; Ambient temperature;

Reference yield:

: 77-17-8
Normeperidine

: 219553-62-5
5-(2-cyanoethoxycarbonyl)-2,6-dimethyl-1,4-dihydro-3-carboxamido>-4-(3,4-methylenedioxyphenyl)pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 83.3 percent / K₂CO₃, KI / dioxane / 24 h / Heating

2: 83 percent / EDC, DMAP / CH₂Cl₂ / 14 h / Ambient temperature

With dmap; potassium carbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; potassium iodide; In 1,4-dioxane; dichloromethane;

Reference yield:

: 4-phenyl-4-piperidinecarboxylic acid 4-methylbenzenesulfonate

: 219553-62-5
5-(2-cyanoethoxycarbonyl)-2,6-dimethyl-1,4-dihydro-3-carboxamido>-4-(3,4-methylenedioxyphenyl)pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / H₂SO₄ / 12 h / Heating

2: 83.3 percent / K₂CO₃, KI / dioxane / 24 h / Heating

3: 83 percent / EDC, DMAP / CH₂Cl₂ / 14 h / Ambient temperature

With dmap; sulfuric acid; potassium carbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; potassium iodide; In 1,4-dioxane; dichloromethane;