5-<(Z)-heptadec-8-en-1-yl>-3-methylthio-1,4-diphenyl-1,2,4-triazolium iodide

Base Information

• Chemical Name: 5-<(Z)-heptadec-8-en-1-yl>-3-methylthio-1,4-diphenyl-1,2,4-triazolium iodide
• CAS No.: 63318-34-3
• Molecular Formula: C₃₂H₄₆N₃S*I
• Molecular Weight: 631.708
• Mol file: 63318-34-3.mol

Synonyms:5-<(Z)-heptadec-8-en-1-yl>-3-methylthio-1,4-diphenyl-1,2,4-triazolium iodide

Chemical Property of 5-<(Z)-heptadec-8-en-1-yl>-3-methylthio-1,4-diphenyl-1,2,4-triazolium iodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-<(Z)-heptadec-8-en-1-yl>-3-methylthio-1,4-diphenyl-1,2,4-triazolium iodide

There total 1 articles about 5-<(Z)-heptadec-8-en-1-yl>-3-methylthio-1,4-diphenyl-1,2,4-triazolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

cis-Octadecenoic acid (112-80-1,2027-47-6) + 3-methyl-1,4-diphenyl isothiosemicarbazide (54211-56-2) → 5-<(Z)-heptadec-8-en-1-yl>-3-methylthio-1,4-diphenyl-1,2,4-triazolium iodide (63318-34-3)

Guidance literature:

With potassium iodide; trichlorophosphate; In pyridine; Heating;

DOI:10.1016/S0040-4020(01)83135-5

Reference yield: 37.0%

5-<(Z)-heptadec-8-en-1-yl>-3-methylthio-1,4-diphenyl-1,2,4-triazolium iodide (63318-34-3) + tetraethyl ammonium → heptadec-8c-enal (56797-41-2) + tetraethylammonium iodide (68-05-3) + 1,4-Diphenyl-3-methylmercapto-1,2,4-triazolium iodide (13136-15-7)

Guidance literature:

With sodium methylate; Yield given. Multistep reaction; 1.) CHCl₃, room temp, 1 h, 2.) MeOH, room temp, 15 min;

DOI:10.1016/S0040-4020(01)83135-5

Reference yield:

5-<(Z)-heptadec-8-en-1-yl>-3-methylthio-1,4-diphenyl-1,2,4-triazolium iodide (63318-34-3) → Oleic aldehyde (2423-10-1)

Guidance literature:

Yield given. Multistep reaction; 1.) NaBH₄ 2.) 1:1 mixture of 38 percent aq. formaldehyde and cc. HCl, 60-70 gradC;

DOI:10.1016/S0040-4039(00)93683-9

upstream raw materials:

cis-Octadecenoic acid

3-methyl-1,4-diphenyl isothiosemicarbazide

Downstream raw materials:

Oleic aldehyde

heptadec-8c-enal

tetraethylammonium iodide

1,4-Diphenyl-3-methylmercapto-1,2,4-triazolium iodide