C₃₁H₅₈O₄Si₂

Base Information

Chemical Name:C₃₁H₅₈O₄Si₂
CAS No.:1261359-90-3
Molecular Formula:C₃₁H₅₈O₄Si₂
Molecular Weight:550.97
Hs Code.:

C<sub>31</sub>H<sub>58</sub>O<sub>4</sub>Si<sub>2</sub>

Synonyms:C₃₁H₅₈O₄Si₂

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Chemical Property of C₃₁H₅₈O₄Si₂

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Technology Process of C₃₁H₅₈O₄Si₂

There total 14 articles about C₃₁H₅₈O₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1261359-76-5
C₁₉H₃₀O₄

: 69739-34-0
t-butyldimethylsiyl triflate

: 1261359-90-3
C₃₁H₅₈O₄Si₂

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at -78 ℃; for 1.5h;
DOI:10.1021/ol1028699

Reference yield:

: 1261359-89-0
C₂₁H₂₆N₄OS

: 1261359-90-3
C₃₁H₅₈O₄Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: ammonium molibdate; dihydrogen peroxide / ethanol / 21 h / 0 °C

2.1: sodium hexamethyldisilazane / 1,2-dimethoxyethane; toluene / 0.08 h / -78 °C

2.2: 1 h / -50 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 16 h / 0 - 20 °C

4.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C

4.2: 2 h / 0 - 20 °C

5.1: AD-mix-β; methanesulfonamide / water; tert-butyl alcohol / 16 h / 0 - 20 °C

5.2: 4 h / 0 °C

6.1: 2,6-dimethylpyridine / dichloromethane / 1.5 h / -78 °C

With 2,6-dimethylpyridine; ammonium molibdate; methanesulfonamide; AD-mix-β; tetrabutyl ammonium fluoride; dihydrogen peroxide; sodium hexamethyldisilazane; sodium hydride; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; dichloromethane; water; toluene; mineral oil; tert-butyl alcohol; 2.1: Julia Olefin synthesis / 2.2: Julia Olefin synthesis;
DOI:10.1021/ol1028699

Reference yield:

: 1261359-72-1
C₂₁H₂₆N₄O₃S

: 1261359-90-3
C₃₁H₅₈O₄Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hexamethyldisilazane / 1,2-dimethoxyethane; toluene / 0.08 h / -78 °C

1.2: 1 h / -50 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 16 h / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C

3.2: 2 h / 0 - 20 °C

4.1: AD-mix-β; methanesulfonamide / water; tert-butyl alcohol / 16 h / 0 - 20 °C

4.2: 4 h / 0 °C

5.1: 2,6-dimethylpyridine / dichloromethane / 1.5 h / -78 °C

With 2,6-dimethylpyridine; methanesulfonamide; AD-mix-β; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; sodium hydride; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; toluene; mineral oil; tert-butyl alcohol; 1.1: Julia Olefin synthesis / 1.2: Julia Olefin synthesis;
DOI:10.1021/ol1028699