(Z)-cyclohex-2-enyl-1-(1-phenyl-1H-imidazol-2-yl)-2-(thiophen-3-yl)vinyl carbonate

Base Information

Chemical Name:(Z)-cyclohex-2-enyl-1-(1-phenyl-1H-imidazol-2-yl)-2-(thiophen-3-yl)vinyl carbonate
CAS No.:1233735-66-4
Molecular Formula:C₂₂H₂₀N₂O₃S
Molecular Weight:392.478
Hs Code.:

Synonyms:(Z)-cyclohex-2-enyl-1-(1-phenyl-1H-imidazol-2-yl)-2-(thiophen-3-yl)vinyl carbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-cyclohex-2-enyl-1-(1-phenyl-1H-imidazol-2-yl)-2-(thiophen-3-yl)vinyl carbonate

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Technology Process of (Z)-cyclohex-2-enyl-1-(1-phenyl-1H-imidazol-2-yl)-2-(thiophen-3-yl)vinyl carbonate

There total 1 articles about (Z)-cyclohex-2-enyl-1-(1-phenyl-1H-imidazol-2-yl)-2-(thiophen-3-yl)vinyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1233735-42-6
1-(1-phenyl-1H-imidazol-2-yl)-2-(thiophen-3-yl)ethan-1-one

: 141037-04-9
cyclohex-2-en-1-yl 1H-imidazole-1-carboxylate

: 1233735-66-4
(Z)-cyclohex-2-enyl-1-(1-phenyl-1H-imidazol-2-yl)-2-(thiophen-3-yl)vinyl carbonate

Guidance literature:: 1-(1-phenyl-1H-imidazol-2-yl)-2-(thiophen-3-yl)ethan-1-one; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.75h; Inert atmosphere;

cyclohex-2-en-1-yl 1H-imidazole-1-carboxylate; With boron trifluoride diethyl etherate; In tetrahydrofuran; 1,2-dimethoxyethane; at -78 ℃; for 0.75h; Inert atmosphere;
DOI:10.1021/ja103771w

Reference yield: 99.0%

: 1233735-66-4
(Z)-cyclohex-2-enyl-1-(1-phenyl-1H-imidazol-2-yl)-2-(thiophen-3-yl)vinyl carbonate

: 1233735-43-7
(S)-2-(cyclohex-2-enyl)-1-(1-phenyl-1H-imidazol-2-yl)-2-(thiophen-3-yl)ethanone

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; (R,R)-ANDEN-phenyl Trost ligand; In 1,4-dioxane; at 20 ℃; for 16h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja103771w