3-(3,5-di-tert-butylphenoxy)propan-1-ol

Base Information

• Chemical Name: 3-(3,5-di-tert-butylphenoxy)propan-1-ol
• CAS No.: 220969-32-4
• Molecular Formula: C₁₇H₂₈O₂
• Molecular Weight: 264.408
• Mol file: 220969-32-4.mol

Synonyms:3-(3,5-di-tert-butylphenoxy)propan-1-ol

Chemical Property of 3-(3,5-di-tert-butylphenoxy)propan-1-ol

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(3,5-di-tert-butylphenoxy)propan-1-ol

There total 1 articles about 3-(3,5-di-tert-butylphenoxy)propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

3,5-Di-tert-butylphenol (1138-52-9) + 1-bromo-3-propanol (627-18-9) → 3-(3,5-di-tert-butylphenoxy)propan-1-ol (220969-32-4)

Guidance literature:

With potassium carbonate; In acetone; Reflux;

DOI:10.1002/anie.201201364

Reference yield: 73.0%

3-(3,5-di-tert-butylphenoxy)propan-1-ol (220969-32-4) + p-toluenesulfonyl chloride (98-59-9) → C24H34O4S (1380401-28-4)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1002/anie.201201364

Reference yield: 72.0%

3-(3,5-di-tert-butylphenoxy)propan-1-ol (220969-32-4) + 2,2,6-trimethyl-4H-1,3-dioxin-4-one (5394-63-8) → 3-(3,5-di-tert-butylphenoxy)propyl 3-oxobutanoate

Guidance literature:

In toluene; at 100 - 110 ℃; for 0.5h; Inert atmosphere;

DOI:10.1016/j.tet.2017.05.035

upstream raw materials:

3,5-Di-tert-butylphenol

1-bromo-3-propanol

Downstream raw materials:

C₁₇H₂₇N₃O

C₅₉H₈₁N₇O₆

C₃₂H₄₆N₄O₄

C₂₇H₃₈N₄O₂