(E)-ethyl 2-[2-(4-chlorobenzylidene)hydrazinyl]-1,3-selenazole-4-carboxylate

Base Information

Chemical Name:(E)-ethyl 2-[2-(4-chlorobenzylidene)hydrazinyl]-1,3-selenazole-4-carboxylate
CAS No.:1450934-25-4
Molecular Formula:C₁₃H₁₂ClN₃O₂Se
Molecular Weight:356.67
Hs Code.:

Synonyms:(E)-ethyl 2-[2-(4-chlorobenzylidene)hydrazinyl]-1,3-selenazole-4-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-ethyl 2-[2-(4-chlorobenzylidene)hydrazinyl]-1,3-selenazole-4-carboxylate

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Technology Process of (E)-ethyl 2-[2-(4-chlorobenzylidene)hydrazinyl]-1,3-selenazole-4-carboxylate

There total 2 articles about (E)-ethyl 2-[2-(4-chlorobenzylidene)hydrazinyl]-1,3-selenazole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 70-23-5
ethyl Bromopyruvate

: 1089306-27-3
C₈H₈ClN₃Se

: 1450934-25-4
(E)-ethyl 2-[2-(4-chlorobenzylidene)hydrazinyl]-1,3-selenazole-4-carboxylate

Guidance literature:: In N,N-dimethyl-formamide; acetone; at 60 ℃; for 1h; Temperature; Time; Microwave irradiation;
DOI:10.3390/molecules18044679

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 1450934-25-4
(E)-ethyl 2-[2-(4-chlorobenzylidene)hydrazinyl]-1,3-selenazole-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol; acetic acid / 4 h / Reflux

2: acetone; N,N-dimethyl-formamide / 1 h / 60 °C / Microwave irradiation

In ethanol; acetic acid; N,N-dimethyl-formamide; acetone;
DOI:10.3390/molecules18044679