N-benzyl-1-(ethylsulfinyl)-N-(4-(methylsulfinyl)butyl)methanamide

Base Information

• Chemical Name: N-benzyl-1-(ethylsulfinyl)-N-(4-(methylsulfinyl)butyl)methanamide
• CAS No.: 1266573-54-9
• Molecular Formula: C₁₅H₂₃NO₃S₂
• Molecular Weight: 329.485
• Mol file: 1266573-54-9.mol

Synonyms:N-benzyl-1-(ethylsulfinyl)-N-(4-(methylsulfinyl)butyl)methanamide

Chemical Property of N-benzyl-1-(ethylsulfinyl)-N-(4-(methylsulfinyl)butyl)methanamide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of N-benzyl-1-(ethylsulfinyl)-N-(4-(methylsulfinyl)butyl)methanamide

There total 2 articles about N-benzyl-1-(ethylsulfinyl)-N-(4-(methylsulfinyl)butyl)methanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.21%

S-ethyl [4-(methylsulfinyl)butyl](phenylmethyl)thiocarbamate → N-benzyl-1-(ethylsulfinyl)-N-(4-(methylsulfinyl)butyl)methanamide (1266573-54-9) + C15H23NO3S2 + C15H23NO4S2

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 - 23 ℃; for 18.5h;

DOI:10.1016/j.bmc.2018.12.026

Reference yield:

4-(methylsulfinyl)butyl methanesulfonate + benzylamine (100-46-9) → N-benzyl-1-(ethylsulfinyl)-N-(4-(methylsulfinyl)butyl)methanamide (1266573-54-9) + C15H23NO3S2 + C15H23NO4S2

Guidance literature:

Multi-step reaction with 2 steps

1.1: ethanol / 0.67 h / 100 °C

1.2: 2 h / 0 - 23 °C

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 18.5 h / -78 - 23 °C

With 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane;

DOI:10.1016/j.bmc.2018.12.026

upstream raw materials:

benzylamine