1-[2-chloro-4-(4-chlorophenoxy)phenyl]-2-(1,2,4-triazol-1-yl)cycloheptanol

Base Information

Chemical Name:1-[2-chloro-4-(4-chlorophenoxy)phenyl]-2-(1,2,4-triazol-1-yl)cycloheptanol
CAS No.:1615678-63-1
Molecular Formula:C₂₁H₂₁Cl₂N₃O₂
Molecular Weight:418.323
Hs Code.:

Synonyms:1-[2-chloro-4-(4-chlorophenoxy)phenyl]-2-(1,2,4-triazol-1-yl)cycloheptanol

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Chemical Property of 1-[2-chloro-4-(4-chlorophenoxy)phenyl]-2-(1,2,4-triazol-1-yl)cycloheptanol

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Technology Process of 1-[2-chloro-4-(4-chlorophenoxy)phenyl]-2-(1,2,4-triazol-1-yl)cycloheptanol

There total 3 articles about 1-[2-chloro-4-(4-chlorophenoxy)phenyl]-2-(1,2,4-triazol-1-yl)cycloheptanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 1615678-81-3
2-chloro-4-(4-chlorophenoxy)-1-iodobenzene

: 100199-07-3
2-(1H-1,2,4-triazol-1-yl)cycloheptanone

: 1615678-63-1
1-[2-chloro-4-(4-chlorophenoxy)phenyl]-2-(1,2,4-triazol-1-yl)cycloheptanol

Guidance literature:: 2-chloro-4-(4-chlorophenoxy)-1-iodobenzene; With bromine; magnesium; In tetrahydrofuran; at 75 ℃; for 1h;

2-(1H-1,2,4-triazol-1-yl)cycloheptanone; With lanthanium (III) chloride bis(lithium chloride) complex; In tetrahydrofuran; at 30 ℃; for 35h;

Reference yield:

: 1056246-49-1
2-bromocycloheptanone

: 1615678-63-1
1-[2-chloro-4-(4-chlorophenoxy)phenyl]-2-(1,2,4-triazol-1-yl)cycloheptanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetone / 3 h / Reflux

2.1: magnesium; bromine / tetrahydrofuran / 1 h / 75 °C

2.2: 35 h / 30 °C

With bromine; potassium carbonate; magnesium; In tetrahydrofuran; acetone;

Reference yield:

: 106-48-9,82344-39-6
4-chloro-phenol

: 101335-11-9
2-chloro-4-fluoro-1-iodobenzene

: 1615678-63-1
1-[2-chloro-4-(4-chlorophenoxy)phenyl]-2-(1,2,4-triazol-1-yl)cycloheptanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 16 h / 95 °C

2.1: magnesium; bromine / tetrahydrofuran / 1 h / 75 °C

2.2: 35 h / 30 °C

With bromine; caesium carbonate; magnesium; In tetrahydrofuran; N,N-dimethyl-formamide;