{(neopentylidene)(2,6-diisopropylphenylimido)(2,6-diisopropylphenoxide)2molybdenum}

Base Information

Chemical Name:{(neopentylidene)(2,6-diisopropylphenylimido)(2,6-diisopropylphenoxide)2molybdenum}
CAS No.:126949-75-5
Molecular Formula:C₄₁H₆₁MoNO₂
Molecular Weight:695.881
Hs Code.:

Synonyms:{(neopentylidene)(2,6-diisopropylphenylimido)(2,6-diisopropylphenoxide)2molybdenum}

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Chemical Property of {(neopentylidene)(2,6-diisopropylphenylimido)(2,6-diisopropylphenoxide)2molybdenum}

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Technology Process of {(neopentylidene)(2,6-diisopropylphenylimido)(2,6-diisopropylphenoxide)2molybdenum}

There total 2 articles about {(neopentylidene)(2,6-diisopropylphenylimido)(2,6-diisopropylphenoxide)2molybdenum} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 72727-49-2
lithium 2,6-diisopropylphenolate

: (neopentylidene)(2,6-diisopropylphenylimido)(1,2-dimethoxy-ethane)(Cl)2 molybdenum

: 126949-75-5
{(neopentylidene)(2,6-diisopropylphenylimido)(2,6-diisopropylphenoxide)2molybdenum}

Guidance literature:: In 1,2-dimethoxyethane; diethyl ether; LiOC6H3(CH(CH3)2)2 is slowly added to soln. of Mo-compd. in ether/dme over 10 min at 30°C, mixt. is allowed to warm to room temp., stirred for 2 h; evapn., extn. (pentane), filtering over Celite, evapn.,recrystn. from pentane (-40°C), elem. anal.;
DOI:10.1021/ja00166a023

Reference yield:

: 108945-97-7
Mo(CHC(CH₃)3)(NC₆H₃(CH(CH₃)2)2)Cl₂

: 126949-75-5
{(neopentylidene)(2,6-diisopropylphenylimido)(2,6-diisopropylphenoxide)2molybdenum}

Guidance literature:: Multi-step reaction with 2 steps

2: diethyl ether; 1,2-dimethoxyethane

In 1,2-dimethoxyethane; diethyl ether;
DOI:10.1021/ja00166a023

Reference yield: 66.0%

: 126949-75-5
{(neopentylidene)(2,6-diisopropylphenylimido)(2,6-diisopropylphenoxide)2molybdenum}

: 754-05-2
ethenyltrimethylsilane

: 127061-14-7,126949-68-6
{(trimethylsilylmethylene)(2,6-diisopropylphenylimido)(2,6-diisopropylphenoxide) molybdenum}

Guidance literature:: In pentane; Mo-compd. is dissolved in pentane and vinyltrimethylsilane is added (25°C), soln. is stirred over night, solvent removed in vac.; conc., standing at -40°C, elem. anal.;
DOI:10.1021/ja00166a023