Technology Process of C39H50O4Si
There total 5 articles about C39H50O4Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: t-BuLi; lithium 2-thienylcyanocuprate / diethyl ether; tetrahydrofuran / -78 - -10 °C
1.2: 91 percent / diethyl ether; tetrahydrofuran / -78 - -30 °C
2.1: 99 percent / aq. TsOH / acetone / Heating
With
tert.-butyl lithium; toluene-4-sulfonic acid; thien-2-yl(cyano)copper lithium;
In
tetrahydrofuran; diethyl ether; acetone;
DOI:10.1016/j.tetlet.2007.01.024
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 63 percent / K2CO3; org. peroxide / benzene / 20 °C
2.1: t-BuLi; lithium 2-thienylcyanocuprate / diethyl ether; tetrahydrofuran / -78 - -10 °C
2.2: 91 percent / diethyl ether; tetrahydrofuran / -78 - -30 °C
3.1: 99 percent / aq. TsOH / acetone / Heating
With
tert.-butyl lithium; potassium carbonate; toluene-4-sulfonic acid; thien-2-yl(cyano)copper lithium;
In
tetrahydrofuran; diethyl ether; acetone; benzene;
DOI:10.1016/j.tetlet.2007.01.024