tert-butyl 2-(tert-butylsulfonyl)-2-(propenyloxycarbonyl)phenylalanylphenylalaninate

Base Information

• Chemical Name: tert-butyl 2-(tert-butylsulfonyl)-2-(propenyloxycarbonyl)phenylalanylphenylalaninate
• CAS No.: 134996-30-8
• Molecular Formula: C₃₀H₄₀N₂O₇S
• Molecular Weight: 572.723

Synonyms:tert-butyl 2-(tert-butylsulfonyl)-2-(propenyloxycarbonyl)phenylalanylphenylalaninate

Chemical Property of tert-butyl 2-(tert-butylsulfonyl)-2-(propenyloxycarbonyl)phenylalanylphenylalaninate

Chemical Property:

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Technology Process of tert-butyl 2-(tert-butylsulfonyl)-2-(propenyloxycarbonyl)phenylalanylphenylalaninate

There total 1 articles about tert-butyl 2-(tert-butylsulfonyl)-2-(propenyloxycarbonyl)phenylalanylphenylalaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.3%

tert-butyl phenylalaninate hydrophosphite + 2-(tert-butylsulfonyl)-2-propenyloxycarbonylphenylalanyl chloride (134996-29-5) → tert-butyl N-(2-(tert-butylsulfonyl)-2-propenyl)phenylalaninate + 2-(t-Butylsulfonyl)-2-propenyloxycarbonyl-L-phenylalanine (134996-41-1) + tert-butyl 2-(tert-butylsulfonyl)-2-propenylphenylalanylphenylalaninate + tert-butyl 2-(tert-butylsulfonyl)-2-(propenyloxycarbonyl)phenylalanylphenylalaninate (134996-30-8)

Guidance literature:

With sodium hydrogencarbonate; In dichloromethane; for 0.166667h; Ambient temperature;

DOI:10.1021/jo982141d

Reference yield: 84.0%

tert-butyl 2-(tert-butylsulfonyl)-2-(propenyloxycarbonyl)phenylalanylphenylalaninate (134996-30-8) → tert-butyl 2-(tert-butylsulfonyl)-2-propenylphenylalanylphenylalaninate

Guidance literature:

With aminomethylpiperidinyl silica gel; In dichloromethane; for 96h;

DOI:10.1021/jo982141d

Reference yield:

tert-butyl 2-(tert-butylsulfonyl)-2-(propenyloxycarbonyl)phenylalanylphenylalaninate (134996-30-8) → (S)-tert-butyl 2-[(S)-2-amino-3-phenylpropanamido]-3-phenylpropanoate (47555-30-6)

Guidance literature:

With 4-Aminomethylpiperidine; In dichloromethane; for 0.25h;

DOI:10.1021/jo982141d

upstream raw materials:

2-(tert-butylsulfonyl)-2-propenyloxycarbonylphenylalanyl chloride

Downstream raw materials:

(S)-tert-butyl 2-[(S)-2-amino-3-phenylpropanamido]-3-phenylpropanoate

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