2,3,4,7a-Tetrahydro-2-methyl-r-1,c-3,5,6,7,t-7a-hexaphenyl-1H-cyclopentapyridin

Base Information

Chemical Name:2,3,4,7a-Tetrahydro-2-methyl-r-1,c-3,5,6,7,t-7a-hexaphenyl-1H-cyclopentapyridin
CAS No.:77951-92-9
Molecular Formula:C₄₅H₃₇N
Molecular Weight:591.795
Hs Code.:

2,3,4,7a-Tetrahydro-2-methyl-r-1,c-3,5,6,7,t-7a-hexaphenyl-1H-cyclopenta<c>pyridin

Synonyms:2,3,4,7a-Tetrahydro-2-methyl-r-1,c-3,5,6,7,t-7a-hexaphenyl-1H-cyclopentapyridin

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Chemical Property of 2,3,4,7a-Tetrahydro-2-methyl-r-1,c-3,5,6,7,t-7a-hexaphenyl-1H-cyclopentapyridin

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Technology Process of 2,3,4,7a-Tetrahydro-2-methyl-r-1,c-3,5,6,7,t-7a-hexaphenyl-1H-cyclopentapyridin

There total 6 articles about 2,3,4,7a-Tetrahydro-2-methyl-r-1,c-3,5,6,7,t-7a-hexaphenyl-1H-cyclopentapyridin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 77951-94-1
2-Methyl-1,3,6,7,8,9-hexaphenyl-2-azoniaspiro<4.4>nona-1,6,8-trien-iodid

: 77951-92-9
2,3,4,7a-Tetrahydro-2-methyl-r-1,c-3,5,6,7,t-7a-hexaphenyl-1H-cyclopentapyridin

Guidance literature:: With sodium tetrahydroborate; In methanol; at -20 ℃;

Reference yield: 76.0%

: 77951-90-7
2,7a-Dihydro-2-methyl-r-1,3,5,6,7,t-7a-hexaphenyl-1H-cyclopentapyridin

: 77951-92-9
2,3,4,7a-Tetrahydro-2-methyl-r-1,c-3,5,6,7,t-7a-hexaphenyl-1H-cyclopentapyridin

Guidance literature:: With hydrogen; platinum(IV) oxide; In chloroform; at 30 ℃; for 10h;

Reference yield:

: 13712-75-9,165618-44-0
3-methyl-2,4-diphenyloxazolium-5-olate

: 77951-92-9
2,3,4,7a-Tetrahydro-2-methyl-r-1,c-3,5,6,7,t-7a-hexaphenyl-1H-cyclopentapyridin

Guidance literature:: Multi-step reaction with 3 steps

1: 33 percent / benzene; acetonitrile / 35 h / Ambient temperature

2: 80 percent / ethanol / 60 h / 70 °C

3: 84 percent / sodium tetrahydroborate / methanol / -20 °C

With sodium tetrahydroborate; In methanol; ethanol; acetonitrile; benzene;