C₂₅H₃₁N₃O₆

Base Information

Chemical Name:C₂₅H₃₁N₃O₆
CAS No.:1338645-91-2
Molecular Formula:C₂₅H₃₁N₃O₆
Molecular Weight:469.538
Hs Code.:

C<sub>25</sub>H<sub>31</sub>N<sub>3</sub>O<sub>6</sub>

Synonyms:C₂₅H₃₁N₃O₆

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Chemical Property of C₂₅H₃₁N₃O₆

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Technology Process of C₂₅H₃₁N₃O₆

There total 13 articles about C₂₅H₃₁N₃O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1338645-90-1
C₄₇H₄₉N₃O₈

: 1338645-91-2
C₂₅H₃₁N₃O₆

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; for 24h;
DOI:10.1021/ol202573s

Reference yield:

: C₂₆H₂₇NO₃

: 1338645-91-2
C₂₅H₃₁N₃O₆

Guidance literature:: Multi-step reaction with 10 steps

1: pyridine / dichloromethane; toluene / -78 - 0 °C

2: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / -78 - 0 °C

3: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone; toluene / 5 h

4: sodium periodate / acetone; toluene / 0.5 h

5: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol

6: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane

7: 1,4-diaza-bicyclo[2.2.2]octane; sodium periodate / tetrahydrofuran; water / 0.17 h

8: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane

9: trifluoroacetic acid / dichloromethane

10: palladium 10% on activated carbon; hydrogen / methanol / 24 h

With pyridine; 1,4-diaza-bicyclo[2.2.2]octane; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; osmium(VIII) oxide; 2-methyl-but-2-ene; palladium 10% on activated carbon; boron trifluoride diethyl etherate; water; hydrogen; benzotriazol-1-ol; 4-methylmorpholine N-oxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; acetone; toluene; tert-butyl alcohol; 5: Pinnick oxidation;
DOI:10.1021/ol202573s

Reference yield:

: C₂₉H₃₃NO₄

: 1338645-91-2
C₂₅H₃₁N₃O₆

Guidance literature:: Multi-step reaction with 7 steps

1: sodium periodate / acetone; toluene / 0.5 h

2: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane

4: 1,4-diaza-bicyclo[2.2.2]octane; sodium periodate / tetrahydrofuran; water / 0.17 h

5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane

6: trifluoroacetic acid / dichloromethane

7: palladium 10% on activated carbon; hydrogen / methanol / 24 h

With 1,4-diaza-bicyclo[2.2.2]octane; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; 2-methyl-but-2-ene; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; acetone; toluene; tert-butyl alcohol; 2: Pinnick oxidation;
DOI:10.1021/ol202573s