C₃₃H₆₀O₄Si₂

Base Information

Chemical Name:C₃₃H₆₀O₄Si₂
CAS No.:1268268-88-7
Molecular Formula:C₃₃H₆₀O₄Si₂
Molecular Weight:577.008
Hs Code.:

C<sub>33</sub>H<sub>60</sub>O<sub>4</sub>Si<sub>2</sub>

Synonyms:C₃₃H₆₀O₄Si₂

Suppliers and Price of C₃₃H₆₀O₄Si₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₃H₆₀O₄Si₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₃H₆₀O₄Si₂

There total 8 articles about C₃₃H₆₀O₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₁H₅₅F₃O₇SSi₂

: 2622-05-1
allylmagnesium bromide

: 1268268-88-7
C₃₃H₆₀O₄Si₂

Guidance literature:: allylmagnesium bromide; With copper(l) iodide; In tetrahydrofuran; at -78 - 0 ℃; for 1h; Inert atmosphere;

C₃₁H₅₅F₃O₇SSi₂; In tetrahydrofuran; at -40 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja200089f

Reference yield:

: 1268268-84-3
C₂₄H₂₈O₄

: 1268268-88-7
C₃₃H₆₀O₄Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: 3,3-dimethyldioxirane / dichloromethane / -78 - 0 °C / Inert atmosphere

1.2: 1.17 h / -78 - 0 °C / Inert atmosphere

1.3: 0 °C

2.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

3.1: diethyl ether; toluene / 0.67 h / -78 - 0 °C / Inert atmosphere

4.1: dmap; triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

5.1: pyridinium p-toluenesulfonate / methanol / 3 h / 65 °C / Inert atmosphere

6.1: 2,6-dimethylpyridine / dichloromethane / 0.25 h / -78 °C / Inert atmosphere

6.2: 0.5 h / -78 - 20 °C / Inert atmosphere

7.1: copper(l) iodide / tetrahydrofuran / 1 h / -78 - 0 °C / Inert atmosphere

7.2: 2 h / -40 °C / Inert atmosphere

With 2,6-dimethylpyridine; dmap; copper(l) iodide; tetrapropylammonium perruthennate; 3,3-dimethyldioxirane; pyridinium p-toluenesulfonate; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene;
DOI:10.1021/ja200089f

Reference yield:

: C₂₈H₃₆O₄

: 1268268-88-7
C₃₃H₆₀O₄Si₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride

2.1: 3,3-dimethyldioxirane / dichloromethane / -78 - 0 °C / Inert atmosphere

2.2: 1.17 h / -78 - 0 °C / Inert atmosphere

2.3: 0 °C

3.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

4.1: diethyl ether; toluene / 0.67 h / -78 - 0 °C / Inert atmosphere

5.1: dmap; triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

6.1: pyridinium p-toluenesulfonate / methanol / 3 h / 65 °C / Inert atmosphere

7.1: 2,6-dimethylpyridine / dichloromethane / 0.25 h / -78 °C / Inert atmosphere

7.2: 0.5 h / -78 - 20 °C / Inert atmosphere

8.1: copper(l) iodide / tetrahydrofuran / 1 h / -78 - 0 °C / Inert atmosphere

8.2: 2 h / -40 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 2,6-dimethylpyridine; dmap; copper(l) iodide; tetrapropylammonium perruthennate; 3,3-dimethyldioxirane; pyridinium p-toluenesulfonate; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene;
DOI:10.1021/ja200089f