N-tert-butyl ester-N-(4-benzylsulfanyl-5-nitro-thiophen-3-ylmethyl)-methanesulfonamide

Base Information

Chemical Name:N-tert-butyl ester-N-(4-benzylsulfanyl-5-nitro-thiophen-3-ylmethyl)-methanesulfonamide
CAS No.:1002761-80-9
Molecular Formula:C₁₈H₂₂N₂O₆S₃
Molecular Weight:458.58
Hs Code.:

Synonyms:N-tert-butyl ester-N-(4-benzylsulfanyl-5-nitro-thiophen-3-ylmethyl)-methanesulfonamide

Suppliers and Price of N-tert-butyl ester-N-(4-benzylsulfanyl-5-nitro-thiophen-3-ylmethyl)-methanesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-tert-butyl ester-N-(4-benzylsulfanyl-5-nitro-thiophen-3-ylmethyl)-methanesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-tert-butyl ester-N-(4-benzylsulfanyl-5-nitro-thiophen-3-ylmethyl)-methanesulfonamide

There total 7 articles about N-tert-butyl ester-N-(4-benzylsulfanyl-5-nitro-thiophen-3-ylmethyl)-methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1002761-79-6
3-benzylsulfanyl-4-chloromethyl-2-nitro-thiophene

: 147751-16-4
tert-butyl (methylsulfonyl)carbamate

: 1002761-80-9
N-tert-butyl ester-N-(4-benzylsulfanyl-5-nitro-thiophen-3-ylmethyl)-methanesulfonamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl acetamide; at 55 ℃; for 16h; Product distribution / selectivity;

Reference yield: 57.0%

: 686271-29-4
(4-benzylsulfanyl-5-nitro-thiophen-3-yl)-methanol

: 147751-16-4
tert-butyl (methylsulfonyl)carbamate

: 1002761-80-9
N-tert-butyl ester-N-(4-benzylsulfanyl-5-nitro-thiophen-3-ylmethyl)-methanesulfonamide

Guidance literature:: With diethylazodicarboxylate; trimethylphosphane; In tetrahydrofuran; toluene; at 25 ℃; for 3.5h;

Reference yield:

: 227312-12-1
5-nitro-4-(phenylmethyl)thio-3-thiophenecarboxylic acid methyl ester

: 1002761-80-9
N-tert-butyl ester-N-(4-benzylsulfanyl-5-nitro-thiophen-3-ylmethyl)-methanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: diisobutylaluminium hydride / dichloromethane / 0.25 h / -40 °C

1.2: 1 h / 25 °C

2.1: trimethylphosphane / tetrahydrofuran / 0.42 h / 25 °C

2.2: 25 °C

With diisobutylaluminium hydride; trimethylphosphane; In tetrahydrofuran; dichloromethane;