1-N-(p-tolylsulfonyl)-3-<2-p-<(tolylsulfonyl)oxy>ethyl>-4-nitro-6,7-dimethoxyindole

Base Information

Chemical Name:1-N-(p-tolylsulfonyl)-3-<2-p-<(tolylsulfonyl)oxy>ethyl>-4-nitro-6,7-dimethoxyindole
CAS No.:153718-72-0
Molecular Formula:C₂₆H₂₆N₂O₉S₂
Molecular Weight:574.632
Hs Code.:

Synonyms:1-N-(p-tolylsulfonyl)-3-<2-p-<(tolylsulfonyl)oxy>ethyl>-4-nitro-6,7-dimethoxyindole

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Chemical Property of 1-N-(p-tolylsulfonyl)-3-<2-p-<(tolylsulfonyl)oxy>ethyl>-4-nitro-6,7-dimethoxyindole

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Technology Process of 1-N-(p-tolylsulfonyl)-3-<2-p-<(tolylsulfonyl)oxy>ethyl>-4-nitro-6,7-dimethoxyindole

There total 1 articles about 1-N-(p-tolylsulfonyl)-3-<2-p-<(tolylsulfonyl)oxy>ethyl>-4-nitro-6,7-dimethoxyindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 153718-68-4
Toluene-4-sulfonic acid 2-[6,7-dimethoxy-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-ethyl ester

: 1-N-(p-tolylsulfonyl)-2-nitro-3-<2-p-<(tolylsulfonyl)oxy>ethyl>-6,7-dimethoxyindole

: 153718-72-0
1-N-(p-tolylsulfonyl)-3-<2-p-<(tolylsulfonyl)oxy>ethyl>-4-nitro-6,7-dimethoxyindole

Guidance literature:: With nitro acetate; acetic anhydride; at -45 - -20 ℃; for 2h;
DOI:10.1021/ja00084a026

Reference yield:

: 153718-72-0
1-N-(p-tolylsulfonyl)-3-<2-p-<(tolylsulfonyl)oxy>ethyl>-4-nitro-6,7-dimethoxyindole

: 153718-74-2
Toluene-4-sulfonic acid 2-[4-amino-6,7-dimethoxy-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-ethyl ester

Guidance literature:: With hydrogen; platinum(IV) oxide; In ethanol; for 0.5h;
DOI:10.1021/ja00084a026

Reference yield:

: 153718-72-0
1-N-(p-tolylsulfonyl)-3-<2-p-<(tolylsulfonyl)oxy>ethyl>-4-nitro-6,7-dimethoxyindole

: 153718-76-4
7-Methoxy-1-<(4-methylphenyl)sulfonyl>-3,4-dihydropyrrolo<4,3,2-de>quinolin-8(1H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / PtO₂ / ethanol / 0.5 h

2: N,N-diisopropylethylamine / CHCl₃ / 1.) 60 deg C, 29 h, 2.) reflux, 24 h

3: 60 percent / aq. ceric ammonium nitrate / acetonitrile / 1 h / 0 °C

With ammonium cerium(IV) nitrate; hydrogen; N-ethyl-N,N-diisopropylamine; platinum(IV) oxide; In ethanol; chloroform; acetonitrile;
DOI:10.1021/ja00084a026