(Z)-2-benzyloxycarbonyl-amino-3-(trimethylsilanyl)acrylic acid methyl ester

Base Information

Chemical Name:(Z)-2-benzyloxycarbonyl-amino-3-(trimethylsilanyl)acrylic acid methyl ester
CAS No.:862693-49-0
Molecular Formula:C₁₅H₂₁NO₄Si
Molecular Weight:307.422
Hs Code.:

Synonyms:(Z)-2-benzyloxycarbonyl-amino-3-(trimethylsilanyl)acrylic acid methyl ester

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Chemical Property of (Z)-2-benzyloxycarbonyl-amino-3-(trimethylsilanyl)acrylic acid methyl ester

Chemical Property:

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Technology Process of (Z)-2-benzyloxycarbonyl-amino-3-(trimethylsilanyl)acrylic acid methyl ester

There total 1 articles about (Z)-2-benzyloxycarbonyl-amino-3-(trimethylsilanyl)acrylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3219-63-4
(trimethylsilyl)methanol

: 100945-15-1,88568-95-0
N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester

: 862693-49-0
(Z)-2-benzyloxycarbonyl-amino-3-(trimethylsilanyl)acrylic acid methyl ester

Guidance literature:: N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 0.5h;

(trimethylsilyl)methanol; With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 ℃;

Reference yield:

: 862693-49-0
(Z)-2-benzyloxycarbonyl-amino-3-(trimethylsilanyl)acrylic acid methyl ester

: 862693-50-3
(R)-2-benzyloxycarbonylamino-3-(trimethylsilanyl)-propionic acid methyl ester

Guidance literature:: With hydrogen; [(1,2,5,6-r)-1,5-cyclooctadiene][(2S,2'S,5 S,5'S)-1,1'-(1,2-phenylene)bis[2,5-diethylphospholane-κP]]-rhodium(1+) trifluoromethanesulfonate; In ethyl acetate; for 2h; under 258.581 Torr;

Reference yield:

: 862693-49-0
(Z)-2-benzyloxycarbonyl-amino-3-(trimethylsilanyl)acrylic acid methyl ester

: 230294-70-9
(R)-2-benzyloxycarbonylamino-3-(trimethylsilanyl)-propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / [(1,2,5,6-r)-1,5-cyclooctadiene][(2S,2'S,5 S,5'S)-1,1'-(1,2-phenylene)bis[2,5-diethylphospholane-κP]]-rhodium(1+) trifluoromethanesulfonate / ethyl acetate / 2 h / 258.58 Torr

2: sodium hydroxide; water / methanol / 2 h / 0 - 20 °C

With sodium hydroxide; water; hydrogen; [(1,2,5,6-r)-1,5-cyclooctadiene][(2S,2'S,5 S,5'S)-1,1'-(1,2-phenylene)bis[2,5-diethylphospholane-κP]]-rhodium(1+) trifluoromethanesulfonate; In methanol; ethyl acetate;