dimethyl 5,5'-[[2-(1-hydroxypropyl)-1,4-phenylene]bis(oxy)]bis[2,2-dimethylpentanoate]

Base Information

Chemical Name:dimethyl 5,5'-[[2-(1-hydroxypropyl)-1,4-phenylene]bis(oxy)]bis[2,2-dimethylpentanoate]
CAS No.:79521-06-5
Molecular Formula:C₂₅H₄₀O₇
Molecular Weight:452.588
Hs Code.:

Synonyms:dimethyl 5,5'-[[2-(1-hydroxypropyl)-1,4-phenylene]bis(oxy)]bis[2,2-dimethylpentanoate]

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Chemical Property of dimethyl 5,5'-[[2-(1-hydroxypropyl)-1,4-phenylene]bis(oxy)]bis[2,2-dimethylpentanoate]

Chemical Property:

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Technology Process of dimethyl 5,5'-[[2-(1-hydroxypropyl)-1,4-phenylene]bis(oxy)]bis[2,2-dimethylpentanoate]

There total 3 articles about dimethyl 5,5'-[[2-(1-hydroxypropyl)-1,4-phenylene]bis(oxy)]bis[2,2-dimethylpentanoate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79520-52-8
5-Bromo-2,2-dimethylpentanoic acid,methyl ester

: 79521-06-5
dimethyl 5,5'-[[2-(1-hydroxypropyl)-1,4-phenylene]bis(oxy)]bis[2,2-dimethylpentanoate]

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, RT, 1 h, 2.) DMF, 80 - 85 deg C, 12 - 14 h

2: NaBH₄ / methanol / Ambient temperature

With sodium tetrahydroborate; sodium hydride; In methanol;
DOI:10.1021/jm00361a015

Reference yield:

: 79521-17-8
dimethyl 5,5'-[[2-(1-oxopropyl)-1,4-phenylene]bis(oxy)]bis[2,2-dimethylpentanoate]

: 79521-06-5
dimethyl 5,5'-[[2-(1-hydroxypropyl)-1,4-phenylene]bis(oxy)]bis[2,2-dimethylpentanoate]

Guidance literature:: With sodium tetrahydroborate; In methanol; Ambient temperature;
DOI:10.1021/jm00361a015

Reference yield:

: 938-46-5
2',5'-dihydroxypropiophenone

: 79521-06-5
dimethyl 5,5'-[[2-(1-hydroxypropyl)-1,4-phenylene]bis(oxy)]bis[2,2-dimethylpentanoate]

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, RT, 1 h, 2.) DMF, 80 - 85 deg C, 12 - 14 h

2: NaBH₄ / methanol / Ambient temperature

With sodium tetrahydroborate; sodium hydride; In methanol;
DOI:10.1021/jm00361a015