(1,1-dimethylethyl)<2-<6-methyl-2-(phenylseleno)bicyclo<3.1.0>hex-3-yl>ethoxy>diphenylsilane

Base Information

Chemical Name:(1,1-dimethylethyl)<2-<6-methyl-2-(phenylseleno)bicyclo<3.1.0>hex-3-yl>ethoxy>diphenylsilane
CAS No.:123827-08-7
Molecular Formula:C₃₁H₃₈OSeSi
Molecular Weight:533.688
Hs Code.:

Synonyms:(1,1-dimethylethyl)<2-<6-methyl-2-(phenylseleno)bicyclo<3.1.0>hex-3-yl>ethoxy>diphenylsilane

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Chemical Property of (1,1-dimethylethyl)<2-<6-methyl-2-(phenylseleno)bicyclo<3.1.0>hex-3-yl>ethoxy>diphenylsilane

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Technology Process of (1,1-dimethylethyl)<2-<6-methyl-2-(phenylseleno)bicyclo<3.1.0>hex-3-yl>ethoxy>diphenylsilane

There total 2 articles about (1,1-dimethylethyl)<2-<6-methyl-2-(phenylseleno)bicyclo<3.1.0>hex-3-yl>ethoxy>diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 2179-79-5
phenyl selenocyanate

: 123826-96-0,133969-92-3,133969-93-4
(1α,2β,3β,5α)-3-<2<<(1,1-dimethylethyl)diphenylsilyl>oxy>ethyl>-6-methylbicyclo<3.1.0>hexan-2-ol

: 123827-08-7
(1,1-dimethylethyl)<2-<6-methyl-2-(phenylseleno)bicyclo<3.1.0>hex-3-yl>ethoxy>diphenylsilane

Guidance literature:: With tributylphosphine; In tetrahydrofuran; for 4h; Ambient temperature;
DOI:10.1021/jo00012a009 DOI:10.1039/c39890000332

Reference yield:

: 123826-95-9,133969-90-1
cis-5-<2<<(1,1-dimethylethyl)diphenylsilyl>oxy>ethyl>-2-cyclopenten-1-ol

: 123827-08-7
(1,1-dimethylethyl)<2-<6-methyl-2-(phenylseleno)bicyclo<3.1.0>hex-3-yl>ethoxy>diphenylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / Sm, HgCl₂ / tetrahydrofuran / from -78 degC to room t.

2: 58 percent / Bu₃P / tetrahydrofuran / 4 h / Ambient temperature

With samarium; tributylphosphine; mercury dichloride; In tetrahydrofuran;
DOI:10.1039/c39890000332

Reference yield: 69.0%

: 123827-08-7
(1,1-dimethylethyl)<2-<6-methyl-2-(phenylseleno)bicyclo<3.1.0>hex-3-yl>ethoxy>diphenylsilane

: 123827-09-8,133969-94-5
cis-(1,1-dimethylethyl)<2-(4-ethyl-2-cyclopenten-1-yl)-ethoxy>diphenylsilane

Guidance literature:: With tri-n-butyl-tin hydride; In hexane; Irradiation; a) 0 -> -10 deg C, 45 min, b) 10 -> 30 deg C, 1.5 h;
DOI:10.1021/jo00012a009