C₃₀H₄₆O₆

Base Information

• Chemical Name: C₃₀H₄₆O₆
• CAS No.: 1119753-98-8
• Molecular Formula: C₃₀H₄₆O₆
• Molecular Weight: 502.692

Synonyms:C₃₀H₄₆O₆

Chemical Property of C₃₀H₄₆O₆

Chemical Property:

Purity/Quality:

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Technology Process of C₃₀H₄₆O₆

There total 1 articles about C₃₀H₄₆O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

C30H48O6 (1119753-96-6) → C30H46O6 (1119753-98-8)

Guidance literature:

With pyridine; Dess-Martin periodane; In dichloromethane; for 0.5h; Inert atmosphere;

DOI:10.1021/ol8027797

Reference yield: 100.0%

S-ethyl propanethioate (2432-42-0) + C30H46O6 (1119753-98-8) → C35H56O7S (1355239-52-9)

Guidance literature:

S-ethyl propanethioate; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

C₃₀H₄₆O₆; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

With ammonium chloride; In tetrahydrofuran; hexane; water; at -78 ℃; Inert atmosphere;

DOI:10.1021/ol203342e

Reference yield:

C30H46O6 (1119753-98-8) → C55H76O10

Guidance literature:

Multi-step reaction with 16 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 °C / Inert atmosphere

1.3: -78 °C / Inert atmosphere

2.1: pyridine / dichloromethane / 2.08 h / 0 - 25 °C / Inert atmosphere

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 0.33 h / 20 - 25 °C / Inert atmosphere

4.1: quinoline; triethylsilane; 1-hexene / dichloromethane / 8 h / 20 - 25 °C / Inert atmosphere

5.1: diethyl ether / 2 h / -78 - 25 °C / Inert atmosphere

5.2: 1 h / Inert atmosphere; Reflux

6.1: lithium hexamethyldisilazane / tetrahydrofuran; toluene / 0.17 h / -78 °C / Inert atmosphere

6.2: 1.5 h / -78 - -20 °C / Inert atmosphere

7.1: N-iodo-succinimide / 1,1,1,3',3',3'-hexafluoro-propanol / 0 °C / Inert atmosphere

8.1: water; potassium carbonate / methanol / 7.5 h / 20 - 25 °C / Inert atmosphere

9.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -10 °C / Inert atmosphere

9.2: 1.5 h / -10 - 25 °C / Inert atmosphere

9.3: 20 - 25 °C / Inert atmosphere

10.1: pyridinium p-toluenesulfonate / dichloromethane / 1 h / 20 - 25 °C / Inert atmosphere

11.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.42 h / -78 °C / Inert atmosphere

11.2: -78 - 0 °C / Inert atmosphere

12.1: tert.-butyl lithium / diethyl ether; pentane / 1.17 h / -78 °C / Inert atmosphere

12.2: 1.03 h / -78 - 0 °C / Inert atmosphere

12.3: Inert atmosphere

13.1: pyridine; Dess-Martin periodane / dichloromethane / 0.25 h / 20 - 25 °C / Inert atmosphere

14.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.75 h / 20 - 25 °C / Inert atmosphere

14.2: 20 - 25 °C / Inert atmosphere

15.1: pyridinium p-toluenesulfonate / dichloromethane / 0.58 h / 0 - 25 °C / Inert atmosphere

16.1: Hoveyda-Grubbs catalyst second generation / 1,2-dichloro-ethane / 24 h / 60 °C / Inert atmosphere

With pyridine; quinoline; triethylsilane; N-iodo-succinimide; n-butyllithium; 1-hexene; Hoveyda-Grubbs catalyst second generation; oxalyl dichloride; tetrabutyl ammonium fluoride; water; tert.-butyl lithium; pyridinium p-toluenesulfonate; potassium carbonate; Dess-Martin periodane; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium hexamethyldisilazane; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; 1,1,1,3',3',3'-hexafluoro-propanol; 1,2-dichloro-ethane; toluene; pentane; 1.2: Aldol addition / 5.1: Soderquist allylation / 11.1: Swern oxidation / 11.2: Swern oxidation / 13.1: Dess-Martin oxidation;

DOI:10.1021/ol203342e

upstream raw materials:

C₃₀H₄₈O₆

Downstream raw materials:

C₃₆H₅₈O₉S₂

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