5-[5-chloro-2-(4-methoxybenzyloxy)benzoyl]-2,3-dimethoxy-[1,4]benzoquinone

Base Information

Chemical Name:5-[5-chloro-2-(4-methoxybenzyloxy)benzoyl]-2,3-dimethoxy-[1,4]benzoquinone
CAS No.:1321576-08-2
Molecular Formula:C₂₃H₁₉ClO₇
Molecular Weight:442.853
Hs Code.:

Synonyms:5-[5-chloro-2-(4-methoxybenzyloxy)benzoyl]-2,3-dimethoxy-[1,4]benzoquinone

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Chemical Property of 5-[5-chloro-2-(4-methoxybenzyloxy)benzoyl]-2,3-dimethoxy-[1,4]benzoquinone

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Technology Process of 5-[5-chloro-2-(4-methoxybenzyloxy)benzoyl]-2,3-dimethoxy-[1,4]benzoquinone

There total 5 articles about 5-[5-chloro-2-(4-methoxybenzyloxy)benzoyl]-2,3-dimethoxy-[1,4]benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1321575-95-4
5-((5-chloro-2-(4-methoxybenzyloxy)phenyl)(hydroxy)methyl)-2,3-dimethoxycyclohexa-2,5-diene-1,4-dione

: 1321576-08-2
5-[5-chloro-2-(4-methoxybenzyloxy)benzoyl]-2,3-dimethoxy-[1,4]benzoquinone

Guidance literature:: With Jones reagent; In acetone; at 0 ℃;
DOI:10.1021/ol201910v

Reference yield:

: 1321575-71-6
1-(5-chloro-2-(4-methoxybenzyloxy)phenyl)prop-2-yn-1-ol

: 1321576-08-2
5-[5-chloro-2-(4-methoxybenzyloxy)benzoyl]-2,3-dimethoxy-[1,4]benzoquinone

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: toluene / 130 °C / Inert atmosphere; Reflux

3.1: Jones reagent / acetone / 0 °C

With Jones reagent; n-butyllithium; In tetrahydrofuran; hexane; acetone; toluene; 2.1: Moore reaction;
DOI:10.1021/ol201910v

Reference yield:

: 632625-64-0
5-chloro-2-((4-methoxybenzyl)oxy)benzaldehyde

: 1321576-08-2
5-[5-chloro-2-(4-methoxybenzyloxy)benzoyl]-2,3-dimethoxy-[1,4]benzoquinone

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrahydrofuran / 3 h / 0 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: toluene / 130 °C / Inert atmosphere; Reflux

4.1: Jones reagent / acetone / 0 °C

With Jones reagent; n-butyllithium; In tetrahydrofuran; hexane; acetone; toluene; 3.1: Moore reaction;
DOI:10.1021/ol201910v