pent-4-enyl 2-azido-2-deoxy-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

Base Information

Chemical Name:pent-4-enyl 2-azido-2-deoxy-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside
CAS No.:206353-05-1
Molecular Formula:C₂₅H₂₉N₃O₅
Molecular Weight:451.522
Hs Code.:

Synonyms:pent-4-enyl 2-azido-2-deoxy-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

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Chemical Property of pent-4-enyl 2-azido-2-deoxy-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

Chemical Property:

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Technology Process of pent-4-enyl 2-azido-2-deoxy-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

There total 5 articles about pent-4-enyl 2-azido-2-deoxy-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 206353-05-1
pent-4-enyl 2-azido-2-deoxy-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / p-TsOH / acetonitrile

2: 97 percent / TfOH / CH₂Cl₂; cyclohexane

3: 1.) ethylenediamine, 2.) DMAP, TfN₃ / 1.) THF, CH₃CN, EtOH, 65 deg C, 2.) CH₃CN, room temperature, overnight

With dmap; trifluorormethanesulfonic acid; triflic azide; toluene-4-sulfonic acid; ethylenediamine; In dichloromethane; cyclohexane; acetonitrile;
DOI:10.1021/jo980427c

Reference yield:

: 182002-91-1
pent-4-enyl 2-deoxy-2-tetrachlorophthalimido-β-D-glucopyranoside

: 206353-05-1
pent-4-enyl 2-azido-2-deoxy-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / p-TsOH / acetonitrile

2: 97 percent / TfOH / CH₂Cl₂; cyclohexane

3: 1.) ethylenediamine, 2.) DMAP, TfN₃ / 1.) THF, CH₃CN, EtOH, 65 deg C, 2.) CH₃CN, room temperature, overnight

With dmap; trifluorormethanesulfonic acid; triflic azide; toluene-4-sulfonic acid; ethylenediamine; In dichloromethane; cyclohexane; acetonitrile;
DOI:10.1021/jo980427c

Reference yield:

: 174356-32-2
pent-4-enyl 4,6-O-benzylidene-2-tetrachlorophthalimido-2-deoxy-β-D-glucopyranoside

: 206353-05-1
pent-4-enyl 2-azido-2-deoxy-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / TfOH / CH₂Cl₂; cyclohexane

2: 1.) ethylenediamine, 2.) DMAP, TfN₃ / 1.) THF, CH₃CN, EtOH, 65 deg C, 2.) CH₃CN, room temperature, overnight

With dmap; trifluorormethanesulfonic acid; triflic azide; ethylenediamine; In dichloromethane; cyclohexane;
DOI:10.1021/jo980427c