Technology Process of C17(14)C2H20N2O3
There total 4 articles about C17(14)C2H20N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
4-benzyloxy-butan-1-ol; C6(14)C2H5FN2O;
With
tetrabutylammomium bromide;
In
tetrahydrofuran;
at 25 ℃;
for 0.5h;
Inert atmosphere;
With
potassium tert-butylate;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 4h;
Inert atmosphere;
DOI:10.3184/174751912X13359587895460
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: copper(l) iodide; 3-hydroxyglutaronitrile; ammonia / methanol / 4 h / 150 °C / Inert atmosphere; Autoclave
2.1: sulfuric acid / 4 h / 0 - 110 °C
3.1: pyridine hydrogenfluoride; sodium nitrite / 3 h / 0 °C / Inert atmosphere
4.1: tetrabutylammomium bromide / tetrahydrofuran / 0.5 h / 25 °C / Inert atmosphere
4.2: 4 h / 0 - 20 °C / Inert atmosphere
With
copper(l) iodide; 3-hydroxyglutaronitrile; sulfuric acid; tetrabutylammomium bromide; ammonia; pyridine hydrogenfluoride; sodium nitrite;
In
tetrahydrofuran; methanol;
DOI:10.3184/174751912X13359587895460
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sulfuric acid / 4 h / 0 - 110 °C
2.1: pyridine hydrogenfluoride; sodium nitrite / 3 h / 0 °C / Inert atmosphere
3.1: tetrabutylammomium bromide / tetrahydrofuran / 0.5 h / 25 °C / Inert atmosphere
3.2: 4 h / 0 - 20 °C / Inert atmosphere
With
sulfuric acid; tetrabutylammomium bromide; pyridine hydrogenfluoride; sodium nitrite;
In
tetrahydrofuran;
DOI:10.3184/174751912X13359587895460
