3,4-di-O-benzyl-2-deoxy-D-erythro-pentose bisbenzyl dithioacetal

Base Information

Chemical Name:3,4-di-O-benzyl-2-deoxy-D-erythro-pentose bisbenzyl dithioacetal
CAS No.:134700-11-1
Molecular Formula:C₃₃H₃₆O₃S₂
Molecular Weight:544.779
Hs Code.:

Synonyms:3,4-di-O-benzyl-2-deoxy-D-erythro-pentose bisbenzyl dithioacetal

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Chemical Property of 3,4-di-O-benzyl-2-deoxy-D-erythro-pentose bisbenzyl dithioacetal

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Technology Process of 3,4-di-O-benzyl-2-deoxy-D-erythro-pentose bisbenzyl dithioacetal

There total 4 articles about 3,4-di-O-benzyl-2-deoxy-D-erythro-pentose bisbenzyl dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 132487-16-2
methyl 3,5-di-O-benzyl-2-deoxy-D-ribofuranoside

: 100-53-8
phenylmethanethiol

: 134700-11-1
3,4-di-O-benzyl-2-deoxy-D-erythro-pentose bisbenzyl dithioacetal

Guidance literature:: With hydrogenchloride;
DOI:10.1016/j.carres.2005.07.011

Reference yield:

: 170984-20-0
Methyl 3,5-di-O-benzyl-2-deoxy-D-erythropentoside

: 100-53-8
phenylmethanethiol

: 134700-11-1
3,4-di-O-benzyl-2-deoxy-D-erythro-pentose bisbenzyl dithioacetal

Guidance literature:: With hydrogenchloride; In chloroform;

Reference yield:

: 452-51-7,13046-70-3,29780-54-9,36792-87-7,36792-88-8,113890-35-0,113890-38-3
D-2-deoxyribose

: 134700-11-1
3,4-di-O-benzyl-2-deoxy-D-erythro-pentose bisbenzyl dithioacetal

Guidance literature:: Multi-step reaction with 3 steps

1: aq. HCl / 0.5 h / Ambient temperature

2: NaH, Bu₄NI / tetrahydrofuran / 60 h / Ambient temperature

3: 85 percent / conc. HCl / 18 h / 40 °C

With hydrogenchloride; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran;
DOI:10.1016/0008-6215(92)84165-O