2-(3-((diphenylmethylene)amino)-5-methyl-2-oxo-2,3-dihydro-1H-imidazol-1-yl)-3-phenylpropanoic acid

Base Information

Chemical Name:2-(3-((diphenylmethylene)amino)-5-methyl-2-oxo-2,3-dihydro-1H-imidazol-1-yl)-3-phenylpropanoic acid
CAS No.:1392506-39-6
Molecular Formula:C₂₆H₂₃N₃O₃
Molecular Weight:425.487
Hs Code.:

Synonyms:2-(3-((diphenylmethylene)amino)-5-methyl-2-oxo-2,3-dihydro-1H-imidazol-1-yl)-3-phenylpropanoic acid

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Chemical Property of 2-(3-((diphenylmethylene)amino)-5-methyl-2-oxo-2,3-dihydro-1H-imidazol-1-yl)-3-phenylpropanoic acid

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Technology Process of 2-(3-((diphenylmethylene)amino)-5-methyl-2-oxo-2,3-dihydro-1H-imidazol-1-yl)-3-phenylpropanoic acid

There total 3 articles about 2-(3-((diphenylmethylene)amino)-5-methyl-2-oxo-2,3-dihydro-1H-imidazol-1-yl)-3-phenylpropanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: (2'RS)-1-((diphenylmethylene)amino)-3-(tert-butyl-3'-phenylpropanoate)-4-methylimidazolin-2-one

: 1392506-39-6
2-(3-((diphenylmethylene)amino)-5-methyl-2-oxo-2,3-dihydro-1H-imidazol-1-yl)-3-phenylpropanoic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 5h; Inert atmosphere;
DOI:10.1021/ol302021n

Reference yield: 69.0%

: (2-(diphenylmethylene)-1-(prop-2-yn-1-yl)hydrazine-1-carbonyl)phenylalanine

: 1392506-39-6
2-(3-((diphenylmethylene)amino)-5-methyl-2-oxo-2,3-dihydro-1H-imidazol-1-yl)-3-phenylpropanoic acid

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; for 12h; Inert atmosphere;
DOI:10.1139/cjc-2019-0479

Reference yield:

: 1392506-36-3
tert-butyl (2-(diphenylmethylene)-1-(prop-2-yn-1-yl)hydrazine-1-carbonyl)-D-phenylalaninate

: 1392506-39-6
2-(3-((diphenylmethylene)amino)-5-methyl-2-oxo-2,3-dihydro-1H-imidazol-1-yl)-3-phenylpropanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / acetonitrile; mineral oil / 2 h / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 5 h / Inert atmosphere

With sodium hydride; trifluoroacetic acid; In dichloromethane; acetonitrile; mineral oil;
DOI:10.1021/ol302021n