4-(1-(2,4-dichlorophenyl)-4-methyl-3-(2-(1-methyl-1H-tetrazol-5-yl)propan-2-ylcarbamoyl)-1H-pyrazol-5-yl)phenyl propane-1-sulfonate

Base Information

Chemical Name:4-(1-(2,4-dichlorophenyl)-4-methyl-3-(2-(1-methyl-1H-tetrazol-5-yl)propan-2-ylcarbamoyl)-1H-pyrazol-5-yl)phenyl propane-1-sulfonate
CAS No.:1331783-58-4
Molecular Formula:C₂₅H₂₇Cl₂N₇O₄S
Molecular Weight:592.506
Hs Code.:

Synonyms:4-(1-(2,4-dichlorophenyl)-4-methyl-3-(2-(1-methyl-1H-tetrazol-5-yl)propan-2-ylcarbamoyl)-1H-pyrazol-5-yl)phenyl propane-1-sulfonate

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Chemical Property of 4-(1-(2,4-dichlorophenyl)-4-methyl-3-(2-(1-methyl-1H-tetrazol-5-yl)propan-2-ylcarbamoyl)-1H-pyrazol-5-yl)phenyl propane-1-sulfonate

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Technology Process of 4-(1-(2,4-dichlorophenyl)-4-methyl-3-(2-(1-methyl-1H-tetrazol-5-yl)propan-2-ylcarbamoyl)-1H-pyrazol-5-yl)phenyl propane-1-sulfonate

There total 2 articles about 4-(1-(2,4-dichlorophenyl)-4-methyl-3-(2-(1-methyl-1H-tetrazol-5-yl)propan-2-ylcarbamoyl)-1H-pyrazol-5-yl)phenyl propane-1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1265634-48-7
C₂₀H₁₈Cl₂N₂O₅S

: 1331783-96-0
2-(1-methyl-1H-tetrazol-5-yl)propan-2-amine

: 1331783-58-4
4-(1-(2,4-dichlorophenyl)-4-methyl-3-(2-(1-methyl-1H-tetrazol-5-yl)propan-2-ylcarbamoyl)-1H-pyrazol-5-yl)phenyl propane-1-sulfonate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 0 - 20 ℃; for 10h;
DOI:10.1016/j.bmcl.2011.06.017

Reference yield:

: 1331783-94-8
benzyl (2-(1-methyl-1H-tetrazol-5-yl)propan-2-yl)carbamate

: 1331783-58-4
4-(1-(2,4-dichlorophenyl)-4-methyl-3-(2-(1-methyl-1H-tetrazol-5-yl)propan-2-ylcarbamoyl)-1H-pyrazol-5-yl)phenyl propane-1-sulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 20% palladium hydroxide on carbon; hydrogen / ethyl acetate / 24 h

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 10 h / 0 - 20 °C

With 20% palladium hydroxide on carbon; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; ethyl acetate;
DOI:10.1016/j.bmcl.2011.06.017