methyl {4'-[3''-(methyl prop-2''(E)-enoate)]phenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid}uronate

Base Information

Chemical Name:methyl {4'-[3''-(methyl prop-2''(E)-enoate)]phenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid}uronate
CAS No.:866417-47-2
Molecular Formula:C₂₃H₂₆O₁₂
Molecular Weight:494.452
Hs Code.:

Synonyms:methyl {4'-[3''-(methyl prop-2''(E)-enoate)]phenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid}uronate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl {4'-[3''-(methyl prop-2''(E)-enoate)]phenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid}uronate

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Technology Process of methyl {4'-[3''-(methyl prop-2''(E)-enoate)]phenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid}uronate

There total 3 articles about methyl {4'-[3''-(methyl prop-2''(E)-enoate)]phenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid}uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 3943-97-3
methyl 4-hydroxycinnamate

: 92420-89-8
methyl 2,3,4-tri-O-acetyl-1-O-(trichloroacetimidoyl)-α-D-glucopyranuronate

: 866417-47-2
methyl {4'-[3''-(methyl prop-2''(E)-enoate)]phenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid}uronate

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1016/j.carres.2005.06.029

Reference yield: 43.0%

: 3943-97-3,19367-38-5,61240-27-5
methyl p-hydroxycinnamate

: 92420-89-8
methyl 2,3,4-tri-O-acetyl-1-O-(trichloroacetimidoyl)-α-D-glucopyranuronate

: 866417-47-2
methyl {4'-[3''-(methyl prop-2''(E)-enoate)]phenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid}uronate

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere; Molecular sieve;
DOI:10.1039/b809965k

Reference yield:

: 7400-08-0,50940-26-6
p-Coumaric Acid

: 866417-47-2
methyl {4'-[3''-(methyl prop-2''(E)-enoate)]phenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid}uronate

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / SOCl₂ / methanol / 48 h / 20 °C

2: 83 percent / BF₃*OEt₂ / CH₂Cl₂ / 16 h / 20 °C

With thionyl chloride; boron trifluoride diethyl etherate; In methanol; dichloromethane;
DOI:10.1016/j.carres.2005.06.029