N¹-benzyloxycarbonyl-N³-tert-butoxycarbonyl-N¹-(2-cyanoethyl)-1,3-propanediamine

Base Information

• Chemical Name: N¹-benzyloxycarbonyl-N³-tert-butoxycarbonyl-N¹-(2-cyanoethyl)-1,3-propanediamine
• CAS No.: 853783-16-1
• Molecular Formula: C₁₉H₂₇N₃O₄
• Molecular Weight: 361.441

Synonyms:N¹-benzyloxycarbonyl-N³-tert-butoxycarbonyl-N¹-(2-cyanoethyl)-1,3-propanediamine

Chemical Property of N¹-benzyloxycarbonyl-N³-tert-butoxycarbonyl-N¹-(2-cyanoethyl)-1,3-propanediamine

Chemical Property:

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Technology Process of N¹-benzyloxycarbonyl-N³-tert-butoxycarbonyl-N¹-(2-cyanoethyl)-1,3-propanediamine

There total 1 articles about N¹-benzyloxycarbonyl-N³-tert-butoxycarbonyl-N¹-(2-cyanoethyl)-1,3-propanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

benzyl chloroformate (501-53-1,94274-21-2) + N1-tert-butoxycarbonyl-N3-(2-cyanoethyl)-1,3-propanediamine (181780-44-9) → N1-benzyloxycarbonyl-N3-tert-butoxycarbonyl-N1-(2-cyanoethyl)-1,3-propanediamine (853783-16-1)

Guidance literature:

With triethylamine; In tetrahydrofuran;

DOI:10.1081/SCC-200054211

Reference yield: 61.0%

N1-benzyloxycarbonyl-N3-tert-butoxycarbonyl-N1-(2-cyanoethyl)-1,3-propanediamine (853783-16-1) → N4-benzyloxycarbonyl-N7-tert-butoxycarbonylnorspermidine (853783-19-4)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃;

DOI:10.1081/SCC-200054211

Reference yield: 54.0%

N1-benzyloxycarbonyl-N3-tert-butoxycarbonyl-N1-(2-cyanoethyl)-1,3-propanediamine (853783-16-1) → 3-{benzyloxycarbonyl-[3-(tert-butoxycarbonylamino)propyl]amino}propionamide (1019333-27-7)

Guidance literature:

With ammonium hydroxide; dihydrogen peroxide; In methanol; at 20 ℃; for 48h;

DOI:10.1080/00397910701845431

upstream raw materials:

benzyl chloroformate

N¹-tert-butoxycarbonyl-N³-(2-cyanoethyl)-1,3-propanediamine

Downstream raw materials:

N⁴-benzyloxycarbonyl-N⁷-tert-butoxycarbonylnorspermidine

3-{benzyloxycarbonyl-[3-(tert-butoxycarbonylamino)propyl]amino}propionamide

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