[5-(ethoxymethoxy)benzene-1,3-diyl]bis[N,N-bis(pyridin-2-ylmethyl)methanamine]

Base Information

• Chemical Name: [5-(ethoxymethoxy)benzene-1,3-diyl]bis[N,N-bis(pyridin-2-ylmethyl)methanamine]
• CAS No.: 1374350-39-6
• Molecular Formula: C₃₅H₃₈N₆O₂
• Molecular Weight: 574.726

Synonyms:[5-(ethoxymethoxy)benzene-1,3-diyl]bis[N,N-bis(pyridin-2-ylmethyl)methanamine]

Chemical Property of [5-(ethoxymethoxy)benzene-1,3-diyl]bis[N,N-bis(pyridin-2-ylmethyl)methanamine]

Chemical Property:

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Technology Process of [5-(ethoxymethoxy)benzene-1,3-diyl]bis[N,N-bis(pyridin-2-ylmethyl)methanamine]

There total 5 articles about [5-(ethoxymethoxy)benzene-1,3-diyl]bis[N,N-bis(pyridin-2-ylmethyl)methanamine] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1,3-bis(chloromethyl)-5-(ethoxymethoxy)benzene (1374350-37-4) + bis[(2-pyridyl)methyl]amine (1539-42-0) → [5-(ethoxymethoxy)benzene-1,3-diyl]bis[N,N-bis(pyridin-2-ylmethyl)methanamine] (1374350-39-6)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 96h;

Reference yield:

dimethyl 5-(ethoxymethoxy)isophthalate (1374350-35-2) → [5-(ethoxymethoxy)benzene-1,3-diyl]bis[N,N-bis(pyridin-2-ylmethyl)methanamine] (1374350-39-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran

2.1: 1,3,5-trichloro-2,4,6-triazine / dichloromethane; N,N-dimethyl-formamide / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h

3.2: 20 °C

With lithium aluminium tetrahydride; 1,3,5-trichloro-2,4,6-triazine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/ejic.201101362

Reference yield:

[5-(ethoxymethoxy)-1,3-phenylene]dimethanol (1374350-36-3) → [5-(ethoxymethoxy)benzene-1,3-diyl]bis[N,N-bis(pyridin-2-ylmethyl)methanamine] (1374350-39-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 1,3,5-trichloro-2,4,6-triazine / dichloromethane; N,N-dimethyl-formamide / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h

2.2: 20 °C

With 1,3,5-trichloro-2,4,6-triazine; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/ejic.201101362

upstream raw materials:

dimethyl 5-(ethoxymethoxy)isophthalate

[5-(ethoxymethoxy)-1,3-phenylene]dimethanol

1,3-bis(chloromethyl)-5-(ethoxymethoxy)benzene

bis[(2-pyridyl)methyl]amine

Downstream raw materials:

3,5-bis{[bis(pyridin-2-ylmethyl)amino]methyl}phenol

((C₅H₄NCH₂)2NCH₂)2C₆H₃OC₃H₆(CH₂COOC(CH₃)3)3(CH₂)8N₄

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