7-(benzyloxy)-2-(3,4-bis(benzyloxy)phenyl)-5-hydroxy-4-oxo-4H-chromen-3-yl 7-(2-(4-(hydroxymethyl)phenylamino)-2-oxoethylamino)-7-oxoheptanoate

Base Information

• Chemical Name: 7-(benzyloxy)-2-(3,4-bis(benzyloxy)phenyl)-5-hydroxy-4-oxo-4H-chromen-3-yl 7-(2-(4-(hydroxymethyl)phenylamino)-2-oxoethylamino)-7-oxoheptanoate
• CAS No.: 1469894-75-4
• Molecular Formula: C₅₂H₄₈N₂O₁₁
• Molecular Weight: 876.96

Synonyms:7-(benzyloxy)-2-(3,4-bis(benzyloxy)phenyl)-5-hydroxy-4-oxo-4H-chromen-3-yl 7-(2-(4-(hydroxymethyl)phenylamino)-2-oxoethylamino)-7-oxoheptanoate

Chemical Property of 7-(benzyloxy)-2-(3,4-bis(benzyloxy)phenyl)-5-hydroxy-4-oxo-4H-chromen-3-yl 7-(2-(4-(hydroxymethyl)phenylamino)-2-oxoethylamino)-7-oxoheptanoate

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Technology Process of 7-(benzyloxy)-2-(3,4-bis(benzyloxy)phenyl)-5-hydroxy-4-oxo-4H-chromen-3-yl 7-(2-(4-(hydroxymethyl)phenylamino)-2-oxoethylamino)-7-oxoheptanoate

There total 1 articles about 7-(benzyloxy)-2-(3,4-bis(benzyloxy)phenyl)-5-hydroxy-4-oxo-4H-chromen-3-yl 7-(2-(4-(hydroxymethyl)phenylamino)-2-oxoethylamino)-7-oxoheptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

7-(benzyloxy)-2-(3,4-bis(benzyloxy)phenyl)-5-hydroxy-4-oxo-4H-chromen-3-yl 7-(2-(4-((tert-butyldiphenylsilyloxy)methyl)phenylamino)-2-oxoethylamino)-7-oxoheptanoate (1469894-71-0) → 7-(benzyloxy)-2-(3,4-bis(benzyloxy)phenyl)-5-hydroxy-4-oxo-4H-chromen-3-yl 7-(2-(4-(hydroxymethyl)phenylamino)-2-oxoethylamino)-7-oxoheptanoate (1469894-75-4)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;

DOI:10.1016/j.bmcl.2013.08.094

Reference yield: 33.0%

7-(benzyloxy)-2-(3,4-bis(benzyloxy)phenyl)-5-hydroxy-4-oxo-4H-chromen-3-yl 7-(2-(4-(hydroxymethyl)phenylamino)-2-oxoethylamino)-7-oxoheptanoate (1469894-75-4) → 2-(3,4-dihydroxyphenyl)-5,7-dihydroxy-4-oxo-4H-chromen-3-yl 7-(2-(4-(hydroxymethyl)phenylamino)-2-oxoethylamino)-7-oxoheptanoate (1469894-60-7)

Guidance literature:

With 5%-palladium/activated carbon; hydrogen; In 1,4-dioxane; ethanol;

DOI:10.1016/j.bmcl.2013.08.094

upstream raw materials:

7-(benzyloxy)-2-(3,4-bis(benzyloxy)phenyl)-5-hydroxy-4-oxo-4H-chromen-3-yl 7-(2-(4-((tert-butyldiphenylsilyloxy)methyl)phenylamino)-2-oxoethylamino)-7-oxoheptanoate

Downstream raw materials:

2-(3,4-dihydroxyphenyl)-5,7-dihydroxy-4-oxo-4H-chromen-3-yl 7-(2-(4-(hydroxymethyl)phenylamino)-2-oxoethylamino)-7-oxoheptanoate

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