2'-{2-[(2S,3R)-3-Hydroxy-2-(2-nitro-phenylsulfanylamino)-butyrylamino]-ethyl}-[2,4']bithiazolyl-4-carboxylic acid (3-methylsulfanyl-propyl)-amide

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Chemical Name:2'-{2-[(2S,3R)-3-Hydroxy-2-(2-nitro-phenylsulfanylamino)-butyrylamino]-ethyl}-[2,4']bithiazolyl-4-carboxylic acid (3-methylsulfanyl-propyl)-amide
CAS No.:82692-06-6
Molecular Formula:C₂₃H₂₈N₆O₅S₄
Molecular Weight:596.777
Hs Code.:

Synonyms:2'-{2-[(2S,3R)-3-Hydroxy-2-(2-nitro-phenylsulfanylamino)-butyrylamino]-ethyl}-[2,4']bithiazolyl-4-carboxylic acid (3-methylsulfanyl-propyl)-amide

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Chemical Property of 2'-{2-[(2S,3R)-3-Hydroxy-2-(2-nitro-phenylsulfanylamino)-butyrylamino]-ethyl}-[2,4']bithiazolyl-4-carboxylic acid (3-methylsulfanyl-propyl)-amide

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Technology Process of 2'-{2-[(2S,3R)-3-Hydroxy-2-(2-nitro-phenylsulfanylamino)-butyrylamino]-ethyl}-[2,4']bithiazolyl-4-carboxylic acid (3-methylsulfanyl-propyl)-amide

There total 3 articles about 2'-{2-[(2S,3R)-3-Hydroxy-2-(2-nitro-phenylsulfanylamino)-butyrylamino]-ethyl}-[2,4']bithiazolyl-4-carboxylic acid (3-methylsulfanyl-propyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 73566-01-5
2,4-dinitrophenyl N-(o-nitrophenylsulfenyl)threoninate

: 78175-36-7
3-[2'-(2-aminoethyl)-2,4'-bithiazole-4-carboxamido]propyl methyl sulfide

: 82692-06-6
2'-{2-[(2S,3R)-3-Hydroxy-2-(2-nitro-phenylsulfanylamino)-butyrylamino]-ethyl}-[2,4']bithiazolyl-4-carboxylic acid (3-methylsulfanyl-propyl)-amide

Guidance literature:: DOI:10.1021/ja00383a045

Reference yield:

: 76275-93-9
methyl 3-<2'-<2-(trifluoroacetamido)ethyl>-2,4'-bithiazole-4-carboxamido>propyl sulfide

: 82692-06-6
2'-{2-[(2S,3R)-3-Hydroxy-2-(2-nitro-phenylsulfanylamino)-butyrylamino]-ethyl}-[2,4']bithiazolyl-4-carboxylic acid (3-methylsulfanyl-propyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / aq. NH₄OH / methanol

2: 68 percent

With ammonium hydroxide; In methanol;
DOI:10.1021/ja00383a045

Reference yield:

: 76275-92-8
2'-<2-(trifluoroacetamido)ethyl>-2,4'-bithiazole-4-carboxylic acid chloride

: 82692-06-6
2'-{2-[(2S,3R)-3-Hydroxy-2-(2-nitro-phenylsulfanylamino)-butyrylamino]-ethyl}-[2,4']bithiazolyl-4-carboxylic acid (3-methylsulfanyl-propyl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / Et₃N, DMAP / CH₂Cl₂

2: 87 percent / aq. NH₄OH / methanol

3: 68 percent

With dmap; ammonium hydroxide; triethylamine; In methanol; dichloromethane;
DOI:10.1021/ja00383a045