Technology Process of C40H51BrN4O9SSi
There total 8 articles about C40H51BrN4O9SSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
carbon tetrabromide; triphenylphosphine;
In
1,2-dichloro-ethane;
for 1h;
DOI:10.1002/hlca.200390244
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 93 percent / pyridine / CH2Cl2 / 3 h / 20 °C
2: 82 percent / Cs2CO3 / dimethylformamide / 4 h / 45 °C
3: oxone; NaOAc / methanol; tetrahydrofuran; H2O
4: 350 mg / oxone; NaOAc / methanol; tetrahydrofuran; H2O / 2 h
5: 99 percent / ZnCl2*Et2O / CH2Cl2
6: 97 percent / PPh3; CBr4 / 1,2-dichloro-ethane / 1 h
With
pyridine; Oxone; zinc chloride diethyl ether; carbon tetrabromide; sodium acetate; caesium carbonate; triphenylphosphine;
In
tetrahydrofuran; methanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.200390244
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 84 percent / Cs2CO3 / tetrahydrofuran / 4 h / 45 °C
2: oxone; NaOAc / methanol; tetrahydrofuran; H2O
3: 350 mg / oxone; NaOAc / methanol; tetrahydrofuran; H2O / 2 h
4: 99 percent / ZnCl2*Et2O / CH2Cl2
5: 97 percent / PPh3; CBr4 / 1,2-dichloro-ethane / 1 h
With
Oxone; zinc chloride diethyl ether; carbon tetrabromide; sodium acetate; caesium carbonate; triphenylphosphine;
In
tetrahydrofuran; methanol; dichloromethane; water; 1,2-dichloro-ethane;
DOI:10.1002/hlca.200390244
