(S)-tert-butyl 1-[allyl(4-methoxyphenyl)-amino]-1-oxopropan-2-ylcarbamate

Base Information

Chemical Name:(S)-tert-butyl 1-[allyl(4-methoxyphenyl)-amino]-1-oxopropan-2-ylcarbamate
CAS No.:950608-94-3
Molecular Formula:C₁₈H₂₆N₂O₄
Molecular Weight:334.415
Hs Code.:

Synonyms:(S)-tert-butyl 1-[allyl(4-methoxyphenyl)-amino]-1-oxopropan-2-ylcarbamate

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Chemical Property of (S)-tert-butyl 1-[allyl(4-methoxyphenyl)-amino]-1-oxopropan-2-ylcarbamate

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Technology Process of (S)-tert-butyl 1-[allyl(4-methoxyphenyl)-amino]-1-oxopropan-2-ylcarbamate

There total 1 articles about (S)-tert-butyl 1-[allyl(4-methoxyphenyl)-amino]-1-oxopropan-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 71954-46-6
N-allyl-4-methoxyaniline

: 15761-38-3
L-N-Boc-Ala

: 950608-94-3
(S)-tert-butyl 1-[allyl(4-methoxyphenyl)-amino]-1-oxopropan-2-ylcarbamate

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1021/ol071241f

Reference yield: 65.0%

: 950608-94-3
(S)-tert-butyl 1-[allyl(4-methoxyphenyl)-amino]-1-oxopropan-2-ylcarbamate

: 950608-95-4
(S)-tert-butyl-1-[allyl(4-methoxyphenyl)amino]-propan-2-ylcarbamate

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃;
DOI:10.1021/ol071241f

Reference yield:

: 950608-94-3
(S)-tert-butyl 1-[allyl(4-methoxyphenyl)-amino]-1-oxopropan-2-ylcarbamate

: 950609-01-5
(S)-N¹-allyl-N²-(4-chlorophenyl)-N¹-(4-methoxyphenyl)propane-1,2-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / lithium aluminum hydride / diethyl ether / 0 °C

2: aq. HCl / dioxane / 2 h / 50 °C

3: 69 percent / sodium tert-butoxide; (+/-)-BINAP / Pd₂(dba)3 / toluene / 80 °C

With hydrogenchloride; lithium aluminium tetrahydride; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In 1,4-dioxane; diethyl ether; toluene;
DOI:10.1021/ol071241f