(6E)-5-[allyl(tert-butylcarbonyl)amino]-1-O-triphenylmethyl-5,6,7-trideoxy-7-phenyl-D-gluco-hept-6-enitol

Base Information

Chemical Name:(6E)-5-[allyl(tert-butylcarbonyl)amino]-1-O-triphenylmethyl-5,6,7-trideoxy-7-phenyl-D-gluco-hept-6-enitol
CAS No.:691905-79-0
Molecular Formula:C₄₀H₄₅NO₆
Molecular Weight:635.8
Hs Code.:

Synonyms:(6E)-5-[allyl(tert-butylcarbonyl)amino]-1-O-triphenylmethyl-5,6,7-trideoxy-7-phenyl-D-gluco-hept-6-enitol

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Chemical Property of (6E)-5-[allyl(tert-butylcarbonyl)amino]-1-O-triphenylmethyl-5,6,7-trideoxy-7-phenyl-D-gluco-hept-6-enitol

Chemical Property:

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Technology Process of (6E)-5-[allyl(tert-butylcarbonyl)amino]-1-O-triphenylmethyl-5,6,7-trideoxy-7-phenyl-D-gluco-hept-6-enitol

There total 5 articles about (6E)-5-[allyl(tert-butylcarbonyl)amino]-1-O-triphenylmethyl-5,6,7-trideoxy-7-phenyl-D-gluco-hept-6-enitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 76-83-5
trityl chloride

: 691905-78-9
(6E)-5-[allyl(tert-butoxycarbonyl)amino]-5,6,7-trideoxy-7-phenyl-D-gluco-hept-6-enitol

: 691905-79-0
(6E)-5-[allyl(tert-butylcarbonyl)amino]-1-O-triphenylmethyl-5,6,7-trideoxy-7-phenyl-D-gluco-hept-6-enitol

Guidance literature:: With pyridine; at 20 ℃; for 18h;
DOI:10.1021/jo049806y

Reference yield:

: 609-06-3
L-xylose

: 691905-79-0
(6E)-5-[allyl(tert-butylcarbonyl)amino]-1-O-triphenylmethyl-5,6,7-trideoxy-7-phenyl-D-gluco-hept-6-enitol

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / ethanol / 16 h / 20 °C

2: 51 percent / triethylamine / acetonitrile; dimethylformamide / 19 h / 0 - 20 °C

3: 68 percent / pyridine / 18 h / 20 °C

With pyridine; triethylamine; In ethanol; N,N-dimethyl-formamide; acetonitrile; 1: Petasis reaction;
DOI:10.1021/jo049806y

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 691905-79-0
(6E)-5-[allyl(tert-butylcarbonyl)amino]-1-O-triphenylmethyl-5,6,7-trideoxy-7-phenyl-D-gluco-hept-6-enitol

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / triethylamine / acetonitrile; dimethylformamide / 19 h / 0 - 20 °C

2: 68 percent / pyridine / 18 h / 20 °C

With pyridine; triethylamine; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo049806y