5-tert-Butyl-2,2-dimethoxy-3-methylene-2-phenyl-2,3-dihydro-2λ⁵-[1,2]oxaphosphole

Base Information

• Chemical Name: 5-tert-Butyl-2,2-dimethoxy-3-methylene-2-phenyl-2,3-dihydro-2λ⁵-[1,2]oxaphosphole
• CAS No.: 78427-01-7
• Molecular Formula: C₁₆H₂₃O₃P
• Molecular Weight: 294.331

Synonyms:5-tert-Butyl-2,2-dimethoxy-3-methylene-2-phenyl-2,3-dihydro-2λ⁵-[1,2]oxaphosphole

Chemical Property of 5-tert-Butyl-2,2-dimethoxy-3-methylene-2-phenyl-2,3-dihydro-2λ⁵-[1,2]oxaphosphole

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Technology Process of 5-tert-Butyl-2,2-dimethoxy-3-methylene-2-phenyl-2,3-dihydro-2λ⁵-[1,2]oxaphosphole

There total 1 articles about 5-tert-Butyl-2,2-dimethoxy-3-methylene-2-phenyl-2,3-dihydro-2λ⁵-[1,2]oxaphosphole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenylphosphonous acid dimethyl ester (2946-61-4) + 2,2-dimethyl-hexa-4,5-dien-3-one (27552-18-7) → 5-tert-Butyl-2,2-dimethoxy-3-methylene-2-phenyl-2,3-dihydro-2λ5-[1,2]oxaphosphole (78427-01-7)

Guidance literature:

In dichloromethane; at -30 ℃; for 3h; Yield given;

DOI:10.1021/ja00405a040

upstream raw materials:

phenylphosphonous acid dimethyl ester

2,2-dimethyl-hexa-4,5-dien-3-one

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