3β-(3'-iodo-4'-aminophenyl)tropane-2β-carboxylic acid methyl ester dihydrochloride

Base Information

• Chemical Name: 3β-(3'-iodo-4'-aminophenyl)tropane-2β-carboxylic acid methyl ester dihydrochloride
• CAS No.: 140633-57-4
• Molecular Formula: C₁₆H₂₁IN₂O₂*2ClH
• Molecular Weight: 473.181

Synonyms:3β-(3'-iodo-4'-aminophenyl)tropane-2β-carboxylic acid methyl ester dihydrochloride

Chemical Property of 3β-(3'-iodo-4'-aminophenyl)tropane-2β-carboxylic acid methyl ester dihydrochloride

Chemical Property:

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Technology Process of 3β-(3'-iodo-4'-aminophenyl)tropane-2β-carboxylic acid methyl ester dihydrochloride

There total 1 articles about 3β-(3'-iodo-4'-aminophenyl)tropane-2β-carboxylic acid methyl ester dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3β-[4'-aminophenyl]tropan-2β-carboxylic acid methyl ester → 3β-(3'-iodo-4'-aminophenyl)tropane-2β-carboxylic acid methyl ester dihydrochloride (140633-57-4)

Guidance literature:

With hydrogenchloride; In glacial AcOH;

Reference yield:

3β-(3'-iodo-4'-aminophenyl)tropane-2β-carboxylic acid methyl ester dihydrochloride (140633-57-4) → 3β-(3-iodo-4-azidophenyl)tropan-2β-carboxylic acid methyl ester

Guidance literature:

With sodium azide; acetic acid; sodium nitrite; Multistep reaction; 1.) 0 deg C, 30 min, 2.) a) 0 deg C, 30 min, b) RT, 30 min;

DOI:10.1021/jm00088a017

Reference yield:

3β-(3'-iodo-4'-aminophenyl)tropane-2β-carboxylic acid methyl ester dihydrochloride (140633-57-4) → RTI 92 (143966-02-3)

Guidance literature:

With phosphoric acid; sodium nitrite; Multistep reaction; 1.) 0 deg C, 30 min, 2.) RT, 2 h;

DOI:10.1021/jm00044a007

Downstream raw materials:

RTI 92

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